3981-79-1

7-十四醇(3981-79-1)核磁图(¹³CNMR)

产品名称:7-十四醇

CAS:3981-79-1

分子式:C14H30O

分子量: 214.39

Mass

MS-KW-0537          
7-tetradecanol
C14H30O             (Mass of molecular ion:    214)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.1
      27.0       5.9
      28.0       1.5
      29.0      13.0
      31.0       2.2
      39.0       3.5
      41.0      25.5
      42.0       5.6
      43.0      33.0
      44.0       5.2
      45.0       2.2
      53.0       1.7
      54.0       2.9
      55.0      91.7
      56.0      12.8
      57.0      22.5
      58.0       4.1
      59.0       1.8
      67.0       4.6
      68.0       4.6
      69.0     100.0
      70.0      14.6
      71.0       7.1
      72.0       1.2
      81.0       3.4
      82.0       3.9
      83.0      14.2
      84.0       6.3
      85.0       4.2
      86.0       1.3
      95.0       1.2
      96.0       3.9
      97.0      78.7
      98.0       8.5
      99.0       1.1
     110.0       2.8
     111.0      35.7
     112.0       4.7
     113.0       2.2
     114.0       2.7
     115.0      33.9
     116.0       2.6
     125.0       1.7
     126.0       1.0
     127.0       1.5
     128.0       1.8
     129.0      29.1
     130.0       2.6
     196.0       5.7
     197.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄H₃₀O	0.038 g : 0.5 ml CDCl₃
7-tetradecanol

    Assign.     Shift(ppm)

     A           3.579
     B           1.50
     C           1.43
     D           1.29
     E           0.89

     Hz     ppm     Int.

   1430.79   3.579     82
    600.96   1.504    116
    577.89   1.446    241
    572.88   1.433    340
    555.42   1.390    138
    514.90   1.288   1000
    359.62   0.900    392
    354.01   0.886    851
    352.79   0.883    900
    346.81   0.868    354

in CDCl3