39905-57-2

4-庚氧基苯胺(39905-57-2)核磁图(¹³CNMR)

产品名称:4-庚氧基苯胺

CAS:39905-57-2

分子式:C12H19NO

分子量: 193.29

Mass

MS-IW-0740          
p-(hexyloxy)aniline
C12H19NO            (Mass of molecular ion:    193)

   Source Temperature: 180 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      27.0       1.7
      28.0       1.6
      29.0       2.0
      39.0       1.6
      41.0       4.6
      42.0       2.3
      43.0       6.8
      53.0       1.9
      55.0       3.4
      56.0       4.5
      57.0       1.0
      65.0       2.0
      69.0       1.6
      80.0       5.6
      81.0       2.6
      92.0       1.3
      94.0       1.2
     108.0      10.0
     109.0     100.0
     110.0       7.4
     193.0      29.3
     194.0       4.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₉ N O	0.040 g : 0.5 ml CDCl₃
p-(hexyloxy)aniline

    Assign.     Shift(ppm)

      A             6.731
      B             6.617
      C             3.865
      D             3.4
      E             1.727
      F             1.43
      G             1.32
      J             0.895

     Hz     ppm     Int.

   2698.73   6.753     57
   2695.31   6.745    667
   2692.99   6.739    233
   2688.72   6.728    272
   2686.40   6.722    935
   2682.98   6.714    118
   2652.10   6.637    111
   2648.68   6.628   1000
   2646.36   6.622    285
   2644.29   6.617     44
   2642.09   6.612    248
   2639.77   6.606    640
   2636.35   6.597     71
   1551.39   3.882    474
   1544.80   3.866    956
   1538.21   3.849    497
   1355.71   3.393     94
    704.96   1.764     95
    698.12   1.747    255
    695.80   1.742     74
    691.16   1.730    306
    689.82   1.727    217
    683.23   1.710    294
    676.64   1.694    132
    586.30   1.468     51
    583.62   1.461     43
    579.35   1.450    134
    577.64   1.446    136
    572.39   1.433    181
    569.95   1.427    167
    566.65   1.418    114
    564.33   1.413    148
    557.25   1.395     76
    548.34   1.373     31
    545.17   1.365     52
    540.89   1.354     89
    539.67   1.351     81
    536.01   1.342    188
    533.81   1.336    565
    530.52   1.328    440
    529.66   1.326    428
    526.61   1.318    658
    523.68   1.311    324
    519.41   1.300    221
    516.85   1.294     81
    514.16   1.287     43
    513.67   1.286     42
    512.70   1.283     48
    365.11   0.914    346
    362.55   0.908    205
    358.15   0.897    911
    355.59   0.890    226
    353.15   0.884    190
    351.07   0.879    300
    346.44   0.867     43

in CDCl3