40175-06-2

1-甲基-1,2,3,6-四氢吡啶-4-羧酸乙酯(40175-06-2)核磁图(¹HNMR)

产品名称:1-甲基-1,2,3,6-四氢吡啶-4-羧酸乙酯

CAS:40175-06-2

分子式:C9H15NO2

分子量: 169.22

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-9994          
ethyl 1-methyl-1,2,3,6-tetrahydro-4-pyridinecarboxylate
C9H15NO2            (Mass of molecular ion:    169)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       2.1
      18.0       1.7
      27.0       5.8
      28.0       2.8
      29.0       4.1
      30.0       1.5
      31.0       1.0
      39.0       2.7
      41.0       4.1
      42.0      24.3
      43.0      15.4
      44.0       8.5
      45.0       1.0
      48.0       1.3
      51.0       1.4
      52.0       1.3
      53.0       8.6
      54.0       1.7
      55.0       2.7
      57.0       1.1
      67.0       2.8
      68.0       2.4
      69.0       3.6
      70.0       3.3
      79.0       1.5
      80.0       2.2
      81.0       8.1
      82.0       2.3
      94.0      17.6
      95.0       3.0
      96.0     100.0
      97.0       8.0
      98.0      10.4
      99.0       4.2
     110.0       1.0
     112.0       2.6
     122.0       3.0
     124.0      15.4
     125.0       1.3
     126.0       1.2
     138.0       3.4
     140.0      32.1
     141.0       2.6
     142.0       1.5
     168.0       4.5
     169.0      13.4
     170.0       2.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₅ N O₂	0.05 ml : 0.5 ml CDCl₃
ethyl 1-methyl-1,2,3,6-tetrahydro-4-pyridinecarboxylate

    Assign.     Shift(ppm)

      A             6.887
      B             4.197
      C             3.09
      D             2.545
      E             2.44
      F             2.371
      G             1.289

     Hz     ppm     Int.

   2757.81   6.901     30
   2756.10   6.897     61
   2754.39   6.893     87
   2752.56   6.888    123
   2750.85   6.884     90
   2749.15   6.879     64
   2747.44   6.875     32
   1688.23   4.225    118
   1681.03   4.207    345
   1673.95   4.189    359
   1666.87   4.171    128
   1240.97   3.106     96
   1237.92   3.098    228
   1234.62   3.090    238
   1231.69   3.082    109
   1024.17   2.563    104
   1017.94   2.548    280
   1012.70   2.534    196
    978.88   2.450     62
    976.44   2.444     82
    973.51   2.436    110
    971.68   2.432    100
    968.75   2.424     69
    966.06   2.418     40
    965.45   2.416     40
    947.75   2.372   1000
    522.34   1.307    370
    515.14   1.289    711
    512.70   1.283     35
    508.06   1.272    390

in CDCl3