4448-75-3

(羟甲基)环庚烷(4448-75-3)质谱(MS)

产品名称:(羟甲基)环庚烷

CAS:4448-75-3

分子式:C8H16O

分子量: 128.21

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-9726          
cycloheptylmethanol
C8H16O              (Mass of molecular ion:    128)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       5.5
      28.0       1.9
      29.0       7.4
      31.0       3.5
      39.0       8.2
      40.0       1.3
      41.0      22.2
      42.0       2.8
      43.0       9.0
      53.0       3.6
      54.0       8.9
      55.0     100.0
      56.0       8.0
      57.0       5.3
      65.0       1.0
      66.0       3.3
      67.0      19.2
      68.0      12.0
      69.0      14.1
      70.0       2.1
      71.0       1.0
      79.0       1.9
      80.0       1.5
      81.0      28.9
      82.0      31.2
      83.0       3.3
      84.0       1.1
      95.0      13.0
      96.0      13.0
      97.0      64.5
      98.0       5.3
     109.0       1.0
     110.0       3.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₆ O	0.05 ml : 0.5 ml CDCl₃
cycloheptylmethanol

    Assign.     Shift(ppm)

      A             3.388
      B             2.43
      C             1.758
      D     *1      1.69
      E     *1      1.63
      F     *2      1.58
      G     *3      1.51
      J     *3      1.43
      K     *2      1.170

     Hz     ppm     Int.

   1357.42   3.397    974
   1350.71   3.380   1000
    971.44   2.431    528
    706.18   1.767    398
    702.51   1.758    403
    699.46   1.751    389
    692.38   1.733    359
    688.84   1.724    462
    686.65   1.719    341
    686.16   1.717    338
    674.93   1.689    386
    672.00   1.682    426
    668.33   1.673    353
    666.26   1.668    364
    665.16   1.665    439
    663.45   1.661    444
    662.48   1.658    441
    659.55   1.651    497
    656.86   1.644    406
    655.76   1.641    378
    652.95   1.634    478
    650.02   1.627    355
    646.36   1.618    319
    643.19   1.610    381
    639.28   1.600    391
    636.60   1.593    402
    632.32   1.583    335
    629.27   1.575    450
    624.88   1.564    453
    611.45   1.530    403
    608.03   1.522    314
    603.88   1.512    362
    602.29   1.508    491
    599.37   1.500    398
    591.80   1.481    559
    590.33   1.478    670
    588.87   1.474    597
    585.69   1.466    382
    581.67   1.456    688
    572.14   1.432    322
    568.85   1.424    355
    484.62   1.213    343
    481.32   1.205    260
    474.73   1.188    555
    471.31   1.180    558
    467.77   1.171    275
    464.84   1.164    297
    461.30   1.155    638
    458.13   1.147    356
    451.66   1.131    290

in CDCl3