454-93-3

3-(fluorosulphonyl)benzoyl chloride (454-93-3)质谱(MS)

产品名称:3-(fluorosulphonyl)benzoyl chloride

CAS:454-93-3

分子式:C7H4ClFO3S

分子量: 222.6212632

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-0586          
m-(fluorosulfonyl)benzoyl chloride
C7H4ClFO3S          (Mass of molecular ion:    222)

   Source Temperature: 270 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       2.2
      36.0       1.2
      37.0       1.1
      38.0       2.9
      50.0      12.7
      51.0       1.3
      52.0       1.0
      63.0       2.6
      64.0       5.0
      73.0       1.2
      74.0       6.2
      75.0      18.4
      76.0      11.1
      80.0       1.4
      83.0       3.2
      92.0      29.2
      93.0       2.1
      95.0       5.2
     104.0       1.5
     111.0       1.4
     159.0      12.8
     187.0     100.0
     188.0       8.6
     189.0       5.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₄ Cl F O₃ S	0.05 ml : 0.5 ml CDCl₃
m-(fluorosulfonyl)benzoyl chloride

    Assign.     Shift(ppm)

      A             8.730
      B             8.561
      C             8.360
      D             7.935

     Hz     ppm     Int.

   3495.64   8.747     22
   3490.75   8.735    581
   3488.92   8.730   1000
   3487.09   8.726    584
   3426.06   8.573    337
   3424.84   8.570    475
   3423.61   8.567    330
   3416.90   8.550    501
   3415.68   8.547    344
   3346.71   8.375    373
   3345.18   8.371    435
   3343.66   8.367    361
   3338.62   8.354    397
   3337.25   8.351    456
   3335.72   8.347    378
   3179.17   7.955    390
   3171.23   7.936    690
   3163.30   7.916    334

in CDCl3

liquid film