4965-33-7

7-氯喹哪啶(4965-33-7)Raman光谱

产品名称:7-氯喹哪啶

CAS:4965-33-7

分子式:C10H8ClN

分子量: 177.63

InChI:InChI=1S/C10H8ClN/c1-7-2-3-8-4-5-9(11)6-10(8)12-7/h2-6H,1H3

InChIKey: WQZQFYRSYLXBGP-UHFFFAOYSA-N

Smiles:N1C2C(=CC=C(Cl)C=2)C=CC=1C

Mass

MS-IW-9006          
7-chloro-2- methylquinoline
C10H8ClN            (Mass of molecular ion:    177)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      38.0       1.1
      39.0       3.2
      50.0       3.8
      51.0       3.7
      52.0       1.0
      57.5       1.4
      61.0       1.1
      62.0       2.2
      63.0       4.1
      64.0       1.0
      68.0       1.3
      70.5       3.6
      73.0       1.3
      74.0       4.0
      75.0       6.2
      75.5       2.2
      76.0       1.9
      86.0       1.1
      87.0       1.6
      88.0       1.6
      88.5       2.6
      89.0       3.2
      98.0       1.0
      99.0       4.1
     100.0       2.2
     101.0       2.3
     102.0       1.2
     110.0       1.0
     113.0       2.5
     114.0       3.4
     115.0      15.2
     116.0       3.8
     126.0       3.0
     127.0       3.7
     135.0       1.6
     136.0       1.1
     140.0       5.8
     141.0       4.5
     142.0      15.9
     143.0       1.8
     149.0       2.1
     150.0       1.0
     151.0       1.9
     162.0       9.1
     163.0       1.1
     164.0       3.0
     176.0       3.5
     177.0     100.0
     178.0      12.4
     179.0      32.3
     180.0       3.7
     191.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₈ Cl N	0.040 g : 0.5 ml CDCl₃
7-chloro-2- methylquinoline

    Assign.     Shift(ppm)

      A             8.002
      B             7.982
      C             7.665
      D             7.407
      E             7.252
      F             2.720

     Hz     ppm     Int.

   3199.22   8.006    147
   3197.27   8.001    156
   3194.21   7.993    141
   3185.67   7.972    131
   3067.99   7.677    143
   3059.33   7.656    169
   2965.33   7.420    110
   2963.26   7.415    110
   2956.67   7.399     95
   2954.59   7.393     93
   2902.71   7.264    188
   2894.29   7.243    180
   1087.28   2.721   1000

in CDCl3