51152-11-5

DL-ISOPINOCAMPHEOL(51152-11-5)核磁图(¹HNMR)

产品名称:DL-ISOPINOCAMPHEOL

CAS:51152-11-5

分子式:C10H18O

分子量: 154.25

Mass

MS-IW-0742          
(+-)-3-pinanol
C10H18O             (Mass of molecular ion:    154)

   Source Temperature: 190 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      18.0       1.7
      27.0       5.7
      29.0       8.0
      31.0       1.1
      39.0       7.3
      40.0       1.2
      41.0      28.0
      42.0       6.5
      43.0      54.9
      44.0       1.7
      45.0       1.0
      51.0       1.4
      53.0       5.2
      54.0       1.7
      55.0      40.6
      56.0       6.0
      57.0       6.4
      58.0       1.7
      65.0       2.1
      67.0      12.5
      68.0       3.8
      69.0      46.3
      70.0     100.0
      71.0      15.2
      72.0       1.5
      77.0       4.5
      79.0       9.5
      80.0       4.6
      81.0      31.8
      82.0       6.8
      83.0      20.9
      84.0      52.1
      85.0       7.4
      91.0       5.0
      92.0       7.1
      93.0      22.8
      94.0       4.9
      95.0      20.6
      96.0       3.8
      97.0       3.0
      98.0      12.2
      99.0       6.4
     105.0       1.8
     107.0       6.1
     108.0       1.4
     110.0       9.0
     111.0       2.8
     121.0      10.9
     122.0       1.1
     136.0       5.2
     137.0       1.1
     139.0       1.2

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₀ H₁₈ O	0.040 g : 0.5 ml DMSO-d₆
(+-)-3-pinanol

    Assign.     Shift(ppm)

      A             4.65
      B             3.817
      C     *1      2.333
      D     *2      2.279
      E             1.86
      F             1.82
      G             1.717
      J     *1      1.619
      K     *3      1.177
      L             1.04
      M     *2      1.01
      N     *3      0.888
     
     ASSIGNED BY C-H AND H-H COSY

     Hz     ppm     Int.

   1862.79   4.662    282
   1857.54   4.648    295
   1533.08   3.837     70
   1528.32   3.825     81
   1523.93   3.814     84
   1518.92   3.801     78
   1513.79   3.788     33
    945.07   2.365     31
    943.85   2.362     31
    941.53   2.356     30
    935.67   2.342     34
    933.72   2.337     42
    931.64   2.332     48
    930.18   2.328     38
    927.86   2.322     35
    921.39   2.306     62
    918.82   2.300     51
    915.28   2.291     68
    912.96   2.285     60
    909.42   2.276     52
    906.01   2.268     71
    903.69   2.262     56
    899.90   2.252     36
    897.58   2.246     31
    746.58   1.869     40
    744.51   1.863     82
    741.33   1.855     84
    738.65   1.849    118
    736.45   1.843     74
    731.45   1.831     82
    729.49   1.826     49
    726.07   1.817     42
    724.12   1.812     54
    692.87   1.734     58
    690.92   1.729     57
    686.89   1.719     98
    684.94   1.714     93
    681.03   1.705     51
    679.08   1.700     47
    657.23   1.645     59
    654.66   1.639     60
    652.34   1.633     62
    649.90   1.627     58
    643.43   1.610     55
    640.87   1.604     55
    638.67   1.599     55
    636.11   1.592     52
    470.34   1.177    940
    418.46   1.048    773
    411.13   1.029    752
    408.45   1.023    213
    399.17   0.999    170
    354.98   0.889   1000

in DMSO-d6

KBr disc

nujol mull

更多供应商

DL-ISOPINOCAMPHEOL(51152-11-5)核磁图(1HNMR)

DL-ISOPINOCAMPHEOL(51152-11-5)核磁图(¹HNMR)