51387-90-7

N-甲基-2-(2-氨乙基)-吡咯烷(51387-90-7)Raman光谱

产品名称:N-甲基-2-(2-氨乙基)-吡咯烷

CAS:51387-90-7

分子式:C7H16N2

分子量: 128.22

Mass

MS-NW-8643          
2-(1-methyl-2-pyrrolidinyl)ethylamine
C7H16N2             (Mass of molecular ion:    128)

   Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      15.0       1.6
      18.0       1.8
      27.0       2.1
      28.0       4.3
      29.0       1.5
      30.0      11.3
      39.0       2.1
      41.0       4.7
      42.0      22.7
      43.0       2.1
      44.0       4.9
      54.0       1.5
      55.0       3.2
      56.0       3.9
      57.0       4.3
      67.0       1.4
      68.0       1.3
      69.0       1.4
      70.0       7.2
      71.0       1.0
      82.0       7.6
      83.0       2.2
      84.0     100.0
      85.0       6.3
      96.0       1.7
      98.0       4.8
     110.0       2.3
     111.0       4.4
     128.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₆ N₂	0.05 ml : 0.5 ml CDCl₃
2-(1-methyl-2-pyrrolidinyl)ethylamine

    Assign.     Shift(ppm)

      A             3.043
      B     *1      2.770
      C     *1      2.679
      D             2.307
      E             2.12
      F             2.06
      G     *2      1.93
      J             1.81
      K     *2      1.68
      L     *3      1.47
      M     *3      1.41

     Hz     ppm     Int.

   1226.07   3.068     52
   1223.88   3.063     57
   1216.55   3.045     96
   1215.09   3.041     78
   1208.98   3.026     55
   1206.91   3.020     59
   1116.70   2.795     46
   1113.28   2.786     46
   1110.11   2.778     76
   1107.79   2.772     55
   1104.49   2.764     77
   1101.07   2.756     79
   1095.46   2.742     74
   1083.01   2.710     66
   1076.66   2.695     74
   1074.34   2.689     77
   1070.80   2.680     44
   1067.87   2.673     73
   1062.13   2.658     45
    922.00   2.308   1000
    859.25   2.151     59
    850.95   2.130     83
    849.85   2.127    121
    841.55   2.106    123
    840.45   2.103    106
    832.15   2.083     91
    827.03   2.070     57
    822.27   2.058     59
    819.09   2.050     64
    787.23   1.970     47
    781.49   1.956     68
    779.54   1.951     71
    777.59   1.946    100
    773.93   1.937    157
    772.09   1.932    165
    769.78   1.927    135
    767.70   1.921     88
    765.38   1.916     80
    764.65   1.914     78
    761.96   1.907     55
    759.77   1.902     62
    757.93   1.897     48
    734.13   1.837     51
    730.96   1.830     62
    728.39   1.823     48
    727.42   1.821     61
    724.61   1.814     63
    721.19   1.805     64
    718.51   1.798     50
    715.45   1.791     53
    714.72   1.789     49
    712.04   1.782     50
    706.79   1.769     45
    703.86   1.762     48
    686.65   1.719     47
    679.20   1.700     50
    672.24   1.683     50
    671.39   1.680     48
    669.31   1.675     51
    591.55   1.481     47
    589.97   1.477     45
    583.13   1.460     45
    580.32   1.453     67
    574.71   1.439     56
    571.41   1.430     74
    567.14   1.420     58
    565.67   1.416     74
    561.77   1.406     52
    558.35   1.398     57
    556.76   1.394     47
    552.61   1.383     51

in CDCl3