5412-69-1

5-二乙基胺基-2-戊醇(5412-69-1)核磁图(¹HNMR)

产品名称:5-二乙基胺基-2-戊醇

CAS:5412-69-1

分子式:C9H21NO

分子量: 159.27

InChI:InChI=1S/C9H21NO/c1-4-10(5-2)8-6-7-9(3)11/h9,11H,4-8H2,1-3H3

InChIKey: OAQYRNDEOJQVBN-UHFFFAOYSA-N

Smiles:CC(O)CCCN(CC)CC

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-5887          
5-diethylamino-2-pentanol
C9H21NO             (Mass of molecular ion:    159)

   Source Temperature: 270 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.5
      27.0       2.9
      28.0       3.0
      29.0       4.2
      30.0       8.5
      41.0       4.2
      42.0       3.9
      43.0       3.8
      44.0       2.3
      45.0       4.3
      56.0       2.9
      57.0       1.4
      58.0      17.6
      69.0       5.5
      70.0       1.1
      71.0       2.1
      72.0       3.5
      73.0       1.1
      74.0       1.4
      84.0       1.4
      85.0       2.7
      86.0     100.0
      87.0       5.8
     144.0       4.3
     159.0       3.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₂₁ N O	0.05 ml : 0.5 ml CDCl₃
5-diethylamino-2-pentanol

    Assign.     Shift(ppm)

      A             3.700
      B     *1      2.632
      C     *1      2.48
      D             2.44
      E             1.7
      F     *2   1.71 to 1.62
      G     *2      1.381
      J             1.157
      K             1.045

     Hz     ppm     Int.

   1487.06   3.721     47
   1484.99   3.716     53
   1480.83   3.706     52
   1478.64   3.700     78
   1476.07   3.694     51
   1472.29   3.684     57
   1469.85   3.678     46
   1070.68   2.680     47
   1063.48   2.662    140
   1057.62   2.647     94
   1056.27   2.643    151
   1050.42   2.629    207
   1049.07   2.625     77
   1043.09   2.611    201
   1035.89   2.592     73
   1007.32   2.521     72
   1000.12   2.503    206
    993.04   2.485    220
    990.11   2.478     50
    987.06   2.470    170
    985.96   2.468    109
    982.18   2.458    114
    979.86   2.452    198
    977.17   2.446    176
    974.61   2.439    127
    972.66   2.434    118
    970.58   2.429    100
    968.63   2.424     46
    966.19   2.418     91
    691.04   1.730     39
    688.48   1.723     40
    687.01   1.720     43
    684.57   1.713     51
    677.73   1.696     58
    675.42   1.691    104
    672.97   1.684     45
    668.58   1.673     58
    664.31   1.663     65
    662.23   1.658     60
    660.52   1.653     60
    660.03   1.652     60
    657.96   1.647     65
    655.52   1.641     60
    653.20   1.635     58
    651.25   1.630     51
    647.34   1.620     54
    646.12   1.617     49
    642.58   1.608     58
    638.92   1.599     34
    637.70   1.596     35
    567.75   1.421     35
    563.48   1.410     33
    558.84   1.399     41
    554.93   1.389     63
    550.42   1.378     34
    546.14   1.367     48
    545.17   1.365     60
    541.75   1.356     33
    536.25   1.342     32
    469.60   1.176     65
    465.70   1.166    619
    459.47   1.150    596
    424.80   1.063    637
    417.60   1.045   1000
    410.28   1.027    585

in CDCl3