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返回ChemicalBook首页>CAS数据库列表>5507-44-8更多图谱> 二乙氧基甲基乙烯基硅烷(5507-44-8)Raman光谱

5507-44-8

二乙氧基甲基乙烯基硅烷(5507-44-8)Raman光谱

分子式:C7H16O2Si

分子量: 160.29

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    Mass

    MS-IW-6964          
    diethoxymethylvinylsilane
    C7H16O2Si           (Mass of molecular ion:    160)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          26.0       1.5
          27.0       2.6
          28.0       2.3
          29.0       1.5
          43.0       2.3
          45.0      11.0
          47.0       1.1
          55.0       1.1
          59.0       1.6
          60.0       1.0
          61.0      14.8
          62.0       1.7
          63.0       7.7
          65.0       1.0
          71.0       6.7
          72.0       1.5
          73.0       7.6
          77.0      15.8
          78.0       1.0
          85.0       1.1
          87.0       5.7
          88.0       1.5
          89.0      22.1
          90.0       1.9
          91.0       4.6
          99.0       1.7
         101.0      29.0
         102.0       2.9
         103.0       2.3
         105.0       9.6
         115.0      20.3
         116.0       2.5
         117.0      10.0
         118.0       1.3
         133.0      16.4
         134.0       1.7
         145.0     100.0
         146.0      11.8
         147.0       4.4
    

parameter in CDCl3

400 MHz in CDCl3

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    1H NMR 300 MHz
    C7 H16 O2 Si 0.05 ml : 0.5 ml CDCl3
    diethoxymethylvinylsilane
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 6.077 D(B) 6.030 D(C) 5.911 J(A,B) 14.8 J(A,C) 5.6 J(B,C) 19.1 D(D) 3.786 D(E) 1.225 J(D,E) 7.2 D(F) 0.196

         Hz     ppm     Int.
    

       1830.50   6.102     32
       1823.57   6.079    190
       1815.92   6.053    159
       1806.46   6.022    191
       1791.78   5.973     55
       1789.91   5.966     17
       1783.09   5.944    139
       1775.61   5.919     91
       1765.88   5.886     50
       1758.29   5.861     39
       1146.66   3.822    160
       1139.46   3.798    490
       1132.31   3.774    500
       1125.11   3.750    170
        374.68   1.249    507
        367.53   1.225    982
        360.32   1.201    489
         58.80   0.196   1000
    

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    1H NMR 399.65 MHz
    C7 H16 O2 Si 0.05 ml : 0.5 ml CDCl3
    diethoxymethylvinylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.08 B 6.06 C 5.911 D 3.786 E 1.225 F 0.196

         Hz     ppm     Int.
    

       2443.73   6.115     33
       2438.11   6.101     63
       2428.96   6.078    178
       2426.03   6.071    143
       2423.46   6.064    186
       2407.96   6.026     38
       2406.86   6.023    205
       2392.09   5.986     92
       2371.09   5.933    166
       2365.48   5.919    140
       2352.05   5.886     76
       2346.44   5.872     71
       1524.29   3.815    202
       1518.68   3.801     51
       1517.21   3.797    543
       1511.72   3.783     52
       1510.13   3.779    586
       1503.17   3.762    253
        496.83   1.244    572
        489.75   1.226   1000
        482.79   1.209    621
         82.40   0.207     60
         78.61   0.197    942
         75.20   0.189     64
    

in CDCl3

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liquid film

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