二乙氧基甲基乙烯基硅烷(5507-44-8)Raman光谱
分子式:C7H16O2Si
分子量: 160.29
InChI:
InChIKey:
Smiles:
-
Mass
MS-IW-6964
diethoxymethylvinylsilane
C7H16O2Si (Mass of molecular ion: 160)
Source Temperature: 220 °C
Sample Temperature: 150 °C
Reservoir, 75 eV
26.0 1.5
27.0 2.6
28.0 2.3
29.0 1.5
43.0 2.3
45.0 11.0
47.0 1.1
55.0 1.1
59.0 1.6
60.0 1.0
61.0 14.8
62.0 1.7
63.0 7.7
65.0 1.0
71.0 6.7
72.0 1.5
73.0 7.6
77.0 15.8
78.0 1.0
85.0 1.1
87.0 5.7
88.0 1.5
89.0 22.1
90.0 1.9
91.0 4.6
99.0 1.7
101.0 29.0
102.0 2.9
103.0 2.3
105.0 9.6
115.0 20.3
116.0 2.5
117.0 10.0
118.0 1.3
133.0 16.4
134.0 1.7
145.0 100.0
146.0 11.8
147.0 4.4
parameter in CDCl3
400 MHz in CDCl3
-
1H NMR |
300 MHz |
C7 H16 O2 Si
|
0.05 ml : 0.5 ml CDCl3
|
diethoxymethylvinylsilane
|
|
Parameter ppm Hz
D(A) 6.077
D(B) 6.030
D(C) 5.911
J(A,B) 14.8
J(A,C) 5.6
J(B,C) 19.1
D(D) 3.786
D(E) 1.225
J(D,E) 7.2
D(F) 0.196
|
Hz ppm Int.
1830.50 6.102 32
1823.57 6.079 190
1815.92 6.053 159
1806.46 6.022 191
1791.78 5.973 55
1789.91 5.966 17
1783.09 5.944 139
1775.61 5.919 91
1765.88 5.886 50
1758.29 5.861 39
1146.66 3.822 160
1139.46 3.798 490
1132.31 3.774 500
1125.11 3.750 170
374.68 1.249 507
367.53 1.225 982
360.32 1.201 489
58.80 0.196 1000
-
1H NMR |
399.65 MHz |
C7 H16 O2 Si
|
0.05 ml : 0.5 ml CDCl3
|
diethoxymethylvinylsilane
|
|
Assign. Shift(ppm)
A 6.08
B 6.06
C 5.911
D 3.786
E 1.225
F 0.196
|
Hz ppm Int.
2443.73 6.115 33
2438.11 6.101 63
2428.96 6.078 178
2426.03 6.071 143
2423.46 6.064 186
2407.96 6.026 38
2406.86 6.023 205
2392.09 5.986 92
2371.09 5.933 166
2365.48 5.919 140
2352.05 5.886 76
2346.44 5.872 71
1524.29 3.815 202
1518.68 3.801 51
1517.21 3.797 543
1511.72 3.783 52
1510.13 3.779 586
1503.17 3.762 253
496.83 1.244 572
489.75 1.226 1000
482.79 1.209 621
82.40 0.207 60
78.61 0.197 942
75.20 0.189 64