Dichloro(p-fluorophenyl)phosphine(5510-93-0)核磁图(¹HNMR)

Parameter ppm Hz D(A) 7.46 D(B) 6.72 J(A,A') 2.5 J(A,B) 8.41 J(A,B') 0.47 J(A,M) 8.38 J(A,X) 5.40 J(A',B) 0.47 J(A',B') 8.41 J(A',M) 8.38 J(A',X) 5.40 J(B,B') 2.4 J(B,M) 1.22 J(B,X) 8.53 J(B',M) 1.22 J(B',X) 8.53 J(M,X) -5.35 BATTERHAM,T.J. & BRAMLEY,R. ORG.MAGN.RESON. 3, 83 (1971)

     Hz     ppm     Int.

   2252.08   7.507     48
   2249.37   7.498    376
   2247.20   7.491    151
   2244.81   7.483    261
   2242.27   7.474    487
   2240.63   7.469    605
   2237.83   7.459    211
   2236.75   7.456    435
   2234.27   7.448    471
   2232.20   7.441    497
   2229.46   7.432    147
   2226.78   7.423    449
   2224.58   7.415     72
   2027.88   6.760     59
   2025.13   6.750    550
   2024.05   6.747    486
   2021.27   6.738    141
   2016.49   6.722    770
   2015.40   6.718   1000
   2012.81   6.709    200
   2009.17   6.697    279
   2008.17   6.694    296
   2006.76   6.689    585
   2004.43   6.681     79