盐酸丙胺(556-53-6)核磁图(¹³CNMR)

Mass

MS-NW-8314          
propylamine hydrochloride
C3H9N HCl           (Mass of molecular ion:     59)

   Source Temperature: 160 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      15.0       1.0
      17.0       1.3
      18.0       7.4
      26.0       1.0
      27.0       3.7
      28.0       9.0
      29.0       2.3
      30.0     100.0
      31.0       1.8
      35.0       4.0
      36.0      32.5
      37.0       1.4
      38.0      10.8
      39.0       2.2
      41.0       6.2
      42.0       3.1
      43.0       2.1
      44.0       1.3
      56.0       1.2
      58.0       2.9
      59.0      14.5

Assign. Shift(ppm) A 8.2 B 2.99 C 1.84 D 1.045

     Hz     ppm     Int.

    735.69   8.215    107
    301.75   3.370     63
    300.69   3.358     64
    298.50   3.333     35
    268.06   2.994    167
    178.56   1.994     31
    175.69   1.962     85
    174.88   1.953     94
    174.06   1.944     89
    172.31   1.924     67
    171.81   1.919     69
    167.56   1.871    174
    163.81   1.830    104
    160.69   1.795    182
    160.25   1.790    183
    156.25   1.745     89
    155.88   1.741     91
    155.38   1.735     91
    153.00   1.709    115
    148.94   1.664     36
    148.25   1.656     34
    147.06   1.643     37
    146.44   1.636     38
    145.94   1.630     39
    145.44   1.624     36
     99.94   1.116    469
     96.50   1.078    117
     93.00   1.039   1000
     85.44   0.954    296
     82.13   0.918     30