5578-42-7

甲基二氯环己基硅烷(5578-42-7)红外图谱(IR1)

产品名称:甲基二氯环己基硅烷

CAS:5578-42-7

分子式:C7H14Cl2Si

分子量: 197.18

InChI:InChI=1S/C7H14Cl2Si/c8-7(9)10-6-4-2-1-3-5-6/h6-7H,1-5,10H2

InChIKey: FRHHUOCGJQERRY-UHFFFAOYSA-N

Smiles:C1([SiH2]C(Cl)Cl)CCCCC1

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-7601          
dichloro(cyclohexyl)methylsilane
C7H14Cl2Si          (Mass of molecular ion:    196)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       3.3
      29.0       2.5
      39.0       5.8
      41.0      16.3
      42.0       1.3
      43.0       1.6
      53.0       3.0
      54.0      12.9
      55.0      61.6
      56.0       3.6
      63.0       5.4
      65.0       2.1
      67.0      31.9
      68.0       1.9
      69.0       1.3
      77.0       1.4
      79.0       3.7
      80.0       2.0
      81.0       8.7
      82.0      80.1
      83.0     100.0
      84.0       7.6
      93.0       1.1
      99.0       1.2
     113.0      28.8
     114.0       2.3
     115.0      19.7
     116.0       1.3
     117.0       4.9
     119.0       1.2
     125.0       1.0
     139.0       1.4
     141.0       1.5
     154.0       4.1
     156.0       2.7
     167.0       2.7
     168.0       1.5
     169.0       2.0
     170.0       1.1
     196.0      13.5
     197.0       1.8
     198.0       9.1
     199.0       1.1
     200.0       1.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₄ Cl₂ Si	0.05 ml : 0.5 ml CDCl₃
dichloro(cyclohexyl)methylsilane

    Assign.     Shift(ppm)

      A             1.87
      B             1.80
      C             1.74
      D             1.26
      E             1.10
      F             0.713

     Hz     ppm     Int.

    752.93   1.884     50
    751.46   1.881     50
    750.00   1.877     44
    748.05   1.872     43
    745.36   1.866     50
    744.02   1.862     53
    741.46   1.856     39
    730.59   1.829     21
    729.00   1.825     24
    727.29   1.820     32
    722.90   1.809     51
    720.58   1.804     67
    719.60   1.801     68
    718.14   1.797     69
    698.61   1.749     32
    697.14   1.745     36
    695.56   1.741     37
    692.14   1.732     33
    690.55   1.728     30
    285.16   0.714   1000

in CDCl3