环丙基甲基氯(5911-08-0)核磁图(¹³CNMR)

Mass

MS-NW-6414          
(chloromethyl)cyclopropane
C4H7Cl              (Mass of molecular ion:     90)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.0
      26.0       6.9
      27.0      32.2
      28.0       8.6
      29.0      22.0
      36.0       1.4
      37.0       1.8
      38.0       3.1
      39.0      27.7
      40.0       2.2
      41.0      27.8
      42.0       1.3
      44.0       1.5
      49.0       2.8
      50.0       3.1
      51.0       3.5
      52.0       1.1
      53.0      11.0
      54.0      19.3
      55.0     100.0
      56.0       4.7
      62.0      27.3
      63.0       1.3
      64.0       9.2
      75.0       6.7
      77.0       2.2
      90.0       2.3

Assign. Shift(ppm) A 3.437 B 1.233 C 0.674 D 0.346

     Hz     ppm     Int.

   1377.44   3.447    963
   1370.00   3.429   1000
    512.82   1.284     31
    508.06   1.272     60
    505.37   1.265     73
    504.88   1.264     69
    503.30   1.260     46
    500.61   1.253    136
    500.00   1.252    138
    497.44   1.245    117
    495.85   1.241     95
    495.36   1.240     85
    492.68   1.233    228
    489.50   1.225     93
    487.79   1.221    125
    485.23   1.215    133
    484.62   1.213    162
    482.06   1.207     45
    479.86   1.201     90
    477.29   1.195     69
    472.53   1.183     36
    279.17   0.699    153
    274.41   0.687    392
    273.19   0.684    473
    272.22   0.682    306
    268.68   0.673    189
    268.19   0.672    196
    266.48   0.667    450
    265.14   0.664    407
    264.28   0.662    318
    260.25   0.652    181
    253.66   0.635     36
    146.85   0.368    176
    142.21   0.356    485
    140.99   0.353    427
    138.43   0.347    240
    137.45   0.344    399
    136.11   0.341    520
    131.59   0.330    136
    131.23   0.329    138
    130.86   0.328    137