5978-08-5

5-氯-2-戊酮乙烯缩酮(5978-08-5)红外图谱(IR1)

产品名称:5-氯-2-戊酮乙烯缩酮

CAS:5978-08-5

分子式:C7H13ClO2

分子量: 164.63

Mass

MS-NW-8659          
2-(3-chloropropyl)-2-methyl-1,3-dioxolane
C7H13ClO2           (Mass of molecular ion:    164)

   Source Temperature: 270 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       3.1
      27.0       5.2
      28.0       2.1
      29.0       3.0
      31.0       1.8
      39.0       6.1
      40.0       1.1
      41.0      13.3
      42.0       4.4
      43.0      58.6
      44.0       2.1
      45.0       2.6
      49.0       1.7
      53.0       1.1
      55.0       5.6
      58.0       2.6
      59.0       1.8
      67.0       2.4
      69.0       1.9
      71.0       2.1
      72.0       3.5
      76.0       1.0
      77.0       7.0
      79.0       2.3
      85.0       4.6
      87.0     100.0
      88.0       4.5
      99.0      10.2
     105.0      12.2
     107.0       4.0
     149.0      30.8
     150.0       2.1
     151.0      10.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₃ Cl O₂	0.05 ml : 0.5 ml CDCl₃
2-(3-chloropropyl)-2-methyl-1,3-dioxolane

    Assign.     Shift(ppm)

      A     *1      3.953
      B     *1      3.926
      C             3.563
      D             1.883
      E             1.788
      F             1.320

     Hz     ppm     Int.

   1590.82   3.981     69
   1589.72   3.978     44
   1583.74   3.963    166
   1581.79   3.958    188
   1579.96   3.954    231
   1578.13   3.949    261
   1576.90   3.946    503
   1572.27   3.935    489
   1571.04   3.932    308
   1569.21   3.927    245
   1567.38   3.922    187
   1565.31   3.917    182
   1559.57   3.903     31
   1558.35   3.900     63
   1432.62   3.585     41
   1430.66   3.580    255
   1429.44   3.577    143
   1426.27   3.569     61
   1424.19   3.564    472
   1417.60   3.548    284
    768.92   1.924     36
    767.58   1.921     42
    762.45   1.908     98
    761.72   1.906     78
    760.74   1.904     96
    757.08   1.895     76
    755.86   1.892    134
    753.54   1.886    127
    752.56   1.884    110
    750.37   1.878    119
    749.27   1.875     98
    746.34   1.868    196
    743.65   1.861     70
    742.07   1.857     32
    740.11   1.852     81
    737.79   1.847     58
    726.93   1.819     32
    722.66   1.809     65
    720.46   1.803    238
    716.43   1.793    138
    713.26   1.785    117
    711.18   1.780    180
    706.05   1.767     81
    704.47   1.763     92
    527.59   1.321   1000

in CDCl3