6052-20-6

4-十六烷基磺酰苯胺(6052-20-6)质谱(MS)

产品名称:4-十六烷基磺酰苯胺

CAS:6052-20-6

分子式:C22H39NO2S

分子量: 381.62

Mass

MS-NW-8055          
p-(hexadecylsulfonyl)aniline
C22H39NO2S          (Mass of molecular ion:    381)

   Source Temperature: 210 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      18.0       1.4
      27.0       1.0
      28.0       1.0
      29.0       4.1
      39.0       1.4
      41.0      10.1
      42.0       1.5
      43.0      13.7
      55.0      10.4
      56.0       1.7
      57.0       7.8
      65.0       4.1
      67.0       1.2
      69.0       5.6
      70.0       1.0
      71.0       2.7
      83.0       3.0
      85.0       1.3
      92.0       8.0
      93.0     100.0
      94.0       9.0
      97.0       1.8
     106.0       2.7
     108.0      11.9
     109.0       1.2
     132.0       1.0
     140.0      15.6
     141.0       2.0
     156.0      11.4
     157.0      38.2
     158.0      12.1
     159.0       2.6
     171.0       2.1
     184.0       1.7
     381.0      26.8
     382.0       7.0
     383.0       2.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₂ H₃₉ N O₂ S	0.031 g : 0.5 ml CDCl₃
p-(hexadecylsulfonyl)aniline

    Assign.     Shift(ppm)

      A             7.635
      B             6.703
      C             4.25
      D             3.017
      E             1.674
      F             1.31
      G             1.25
      J             1.23
      K             0.877

     Hz     ppm     Int.

   3058.59   7.654     37
   3055.91   7.647    284
   3053.96   7.642     97
   3049.19   7.630     96
   3047.24   7.625    300
   3044.56   7.619     44
   2686.04   6.721     41
   2683.47   6.715    332
   2681.40   6.710    106
   2676.64   6.698    100
   2674.68   6.693    307
   2672.00   6.686     45
   1698.73   4.251    187
   1214.48   3.039    148
   1209.11   3.026     73
   1206.42   3.019    108
   1203.98   3.013     67
   1203.13   3.011     69
   1198.24   2.999    157
    678.83   1.699     60
    677.61   1.696     56
    674.32   1.688     79
    670.90   1.679     99
    666.87   1.669     58
    663.21   1.660     77
    660.40   1.653     42
    655.15   1.640     38
    536.38   1.343     52
    535.52   1.340     52
    535.16   1.340     51
    528.81   1.324     85
    527.47   1.320     84
    526.49   1.318     86
    526.25   1.317     86
    519.29   1.300    104
    511.60   1.281    120
    500.85   1.254   1000
    490.11   1.227    862
    357.91   0.896    147
    351.20   0.879    454
    344.12   0.862    182

in DMSO-d6

KBr disc

nujol mull