6088-51-3

双(6-羟基-2-萘)二硫(6088-51-3)质谱(MS)

产品名称:双(6-羟基-2-萘)二硫

CAS:6088-51-3

分子式:C20H14O2S2

分子量: 350.45

InChI:InChI=1S/C20H14O2S2/c21-17-5-1-15-11-19(7-3-13(15)9-17)23-24-20-8-4-14-10-18(22)6-2-16(14)12-20/h1-12,21-22H

InChIKey: AHXGXXJEEHFHDK-UHFFFAOYSA-N

Smiles:S(C1C=CC2C(C=1)=CC=C(O)C=2)SC1C=CC2C(C=1)=CC=C(O)C=2

Mass

MS-NW-2410          
6,6'-dithiodi-2-naphthol
C20H14O2S2          (Mass of molecular ion:    350)

   Source Temperature: 230 °C
   Sample Temperature: 190 °C
   Direct, 75 eV

      17.0       2.3
      18.0      10.8
      28.0       3.3
      39.0       2.1
      43.0       1.0
      45.0       3.1
      50.0       1.5
      51.0       3.2
      62.0       1.8
      63.0       3.7
      65.0       1.0
      69.0       2.9
      73.0       1.0
      74.0       1.5
      75.0       2.0
      76.0       1.4
      77.0       7.1
      79.0       1.2
      87.0       2.5
      88.0       3.6
      89.0       1.8
      93.0       1.1
     102.0       7.0
     103.0       7.8
     113.0       1.4
     114.0       1.8
     115.0      30.0
     116.0       4.7
     131.0      35.2
     132.0       5.5
     143.0       2.1
     144.0      12.5
     145.0       3.5
     146.0       1.6
     147.0      12.8
     148.0       3.4
     158.0       1.5
     174.0       1.6
     175.0      46.3
     176.0     100.0
     177.0      13.1
     178.0       5.3
     286.0       1.1
     350.0      10.7
     351.0       2.6
     352.0       1.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₂₀ H₁₄ O₂ S₂	0.036 g : 0.5 ml DMSO-d₆
6,6'-dithiodi-2-naphthol

    Assign.     Shift(ppm)

      A             9.97
      B             7.979
      C             7.744
      D             7.728
      E             7.537
      F             7.18
      G             7.14

     Hz     ppm     Int.

   3996.14  10.000     49
   3995.59   9.998     51
   3994.68   9.996     61
   3993.76   9.994     69
   3993.03   9.992     78
   3991.38   9.988    107
   3985.89   9.974    303
   3985.52   9.973    299
   3981.49   9.963    128
   3981.12   9.962    114
   3978.38   9.955     65
   3977.83   9.954     56
   3190.03   7.983    765
   3188.20   7.978    775
   3105.04   7.770     52
   3104.67   7.769     57
   3104.31   7.768     68
   3103.94   7.767     68
   3103.02   7.765     76
   3099.91   7.757    635
   3096.06   7.747    109
   3092.95   7.740    731
   3091.30   7.736    743
   3087.64   7.726    109
   3084.52   7.719    775
   3081.04   7.710     53
   3017.30   7.550    610
   3015.29   7.545    582
   3012.36   7.538     60
   3011.44   7.536     64
   3011.07   7.535     69
   3010.52   7.533     78
   3008.51   7.528    510
   3006.68   7.524    486
   2863.44   7.165     55
   2862.53   7.163     67
   2858.68   7.153    530
   2856.66   7.148   1000
   2854.83   7.144    866
   2852.27   7.137    306
   2850.80   7.134    107
   2849.89   7.131     86
   2849.34   7.130     85
   2846.04   7.122    604
   2843.66   7.116    433

in DMSO-d6