4-羟基-3-(Α-亚氨基苄基)-1-甲基-6-苯基吡啶-2(1H)-酮(60986-58-5)核磁图(¹³CNMR)

Mass

MS-NW-9927          
4-hydroxy-3-(alpha-iminobenzyl)-1-methyl-6-phenyl-2(1H)-pyridinone
C19H16N2O2          (Mass of molecular ion:    304)

   Source Temperature: 170 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      17.0       1.0
      18.0       5.3
      28.0       1.1
      51.0       2.3
      58.0       1.2
      76.0       1.9
      77.0       8.6
      78.0       1.0
      82.0       2.4
      89.0       1.7
      90.0       1.5
      91.0       2.9
     102.0       2.3
     103.0       7.1
     104.0       4.7
     105.0       1.2
     115.0       1.6
     116.0       1.4
     117.0       2.4
     118.0       9.2
     129.0       1.5
     130.0       2.0
     131.0       1.1
     132.0       2.3
     138.0       1.9
     144.0       2.1
     146.0       1.5
     151.0       3.9
     152.0       2.3
     158.0       4.5
     160.0       1.9
     172.0       1.2
     200.0      10.0
     201.0       5.2
     227.0       2.4
     260.0       1.2
     276.0       1.4
     289.0       4.3
     303.0     100.0
     304.0      34.2
     305.0       5.7

Assign. Shift(ppm) A *1 13. B *1 7.5 C *2 7.44 D *2 7.39 E *3 7.32 F *3 7.31 G 5.62 J 2.937

     Hz     ppm     Int.

   2982.68   7.464     94
   2981.40   7.461    163
   2980.49   7.458    158
   2978.47   7.453    621
   2976.27   7.448    424
   2974.62   7.444    852
   2971.88   7.437   1000
   2968.03   7.427    142
   2958.14   7.402    653
   2955.57   7.396    717
   2951.54   7.386    661
   2948.98   7.379    235
   2936.34   7.348    114
   2933.05   7.340    492
   2930.85   7.334    493
   2927.37   7.325    777
   2924.99   7.319    448
   2923.70   7.316    680
   2920.22   7.307    418
   2917.84   7.301    361
   2244.34   5.616     98
   1173.18   2.936    419