61-49-4

N(omega)-甲基色胺(61-49-4)红外图谱(IR1)

产品名称:N(omega)-甲基色胺

CAS:61-49-4

分子式:C11H14N2

分子量: 174.24

InChI:InChI=1S/C11H14N2/c1-12-7-6-9-8-13-11-5-3-2-4-10(9)11/h2-5,8,12-13H,6-7H2,1H3

InChIKey: NCIKQJBVUNUXLW-UHFFFAOYSA-N

Smiles:N1C2=C(C=CC=C2)C(CCNC)=C1

Mass

MS-NW-8073          
2-(3-indolyl)-N-methylethylamine
C11H14N2            (Mass of molecular ion:    174)

   Source Temperature: 160 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      18.0       2.2
      28.0       1.7
      39.0       1.0
      42.0       2.0
      44.0      91.5
      45.0       2.4
      51.0       1.8
      63.0       1.4
      76.0       1.2
      77.0       8.0
      78.0       1.0
      89.0       1.4
     102.0       2.7
     103.0       6.6
     115.0       2.4
     117.0       1.7
     128.0       2.0
     129.0       1.8
     130.0      57.1
     131.0     100.0
     132.0      10.7
     143.0       2.0
     144.0       1.9
     174.0      10.4
     175.0       2.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₄ N₂	0.035 g : 0.5 ml CDCl₃
2-(3-indolyl)-N-methylethylamine

    Assign.     Shift(ppm)

      A             8.82
      B             7.626
      C             7.311
      D             7.181
      E             7.109
      F             6.961
      G     *1      2.985
      J     *1      2.927
      K             2.436
      L             1.38

     Hz     ppm     Int.

   3526.37   8.824     35
   3051.88   7.637    123
   3044.07   7.617    131
   2927.25   7.325     91
   2926.39   7.323    133
   2925.54   7.321     87
   2919.19   7.305    123
   2918.33   7.303    186
   2917.48   7.301    113
   2878.17   7.202     67
   2877.08   7.200     71
   2871.22   7.185    112
   2870.00   7.182    136
   2863.16   7.165     86
   2861.94   7.162     79
   2848.39   7.128    113
   2847.29   7.125    112
   2841.31   7.110     91
   2840.45   7.108    155
   2839.48   7.105    110
   2833.50   7.090     70
   2832.40   7.088     64
   2781.98   6.962    177
   1201.29   3.006     45
   1199.71   3.002     51
   1199.10   3.001     50
   1193.24   2.986    201
   1187.38   2.972    196
   1175.66   2.942    164
   1169.68   2.927    187
   1166.99   2.921     71
   1163.33   2.911     51
   1161.13   2.906     44
    973.63   2.437   1000

in CDCl3