612-17-9

1,4-二羟基萘(612-17-9)核磁图(¹³CNMR)

产品名称:1,4-二羟基萘

CAS:612-17-9

分子式:C10H10

分子量: 130.19

InChI:InChI=1S/C10H10/c1-2-6-10-8-4-3-7-9(10)5-1/h1-6H,7-8H2

InChIKey: FUPIVZHYVSCYLX-UHFFFAOYSA-N

Smiles:C1C2=C(C=CC=C2)CC=C1

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-3095          
1,4-dihydronaphthalene
C10H10              (Mass of molecular ion:    130)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      27.0       1.8
      38.0       1.1
      39.0       4.5
      50.0       4.2
      51.0      10.4
      52.0       2.1
      62.0       1.9
      63.0       7.1
      63.5       2.7
      64.0       9.4
      64.5       2.3
      65.0       3.8
      74.0       2.9
      75.0       3.2
      76.0       2.5
      77.0       6.6
      78.0       3.3
      89.0       2.1
      91.0       4.8
     101.0       2.0
     102.0       5.6
     103.0       2.4
     104.0       8.6
     115.0      37.6
     116.0       4.1
     117.0       1.4
     126.0       3.5
     127.0      16.9
     128.0      44.7
     129.0      73.8
     130.0     100.0
     131.0      11.3
     132.0       5.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₀	0.05 ml : 0.5 ml CDCl₃
1,4-dihydronaphthalene

    Assign.     Shift(ppm)

      A             7.09
      B             5.883
      C             3.349

     Hz     ppm     Int.

    644.31   7.195     23
    637.88   7.123     73
    634.94   7.090   1000
    627.50   7.007     23
    625.44   6.984     25
    531.19   5.932     43
    530.19   5.920     64
    528.56   5.902    237
    527.00   5.885    607
    525.56   5.869    270
    524.38   5.856     72
    522.94   5.839     49
    302.38   3.377     72
    300.69   3.358    832
    299.25   3.342    805
    297.56   3.323    112
    296.69   3.313     74

in CDCl3