赖氨酸二盐酸盐(617-68-5)红外图谱(IR1)
分子式:C6H16Cl2N2O2
分子量: 219.11
InChI:InChI=1S/C6H14N2O2.2ClH/c7-4-2-1-3-5(8)6(9)10;;/h5H,1-4,7-8H2,(H,9,10);2*1H
InChIKey: JBBURJFZIMRPCZ-UHFFFAOYSA-N
Smiles:C(N)(C(=O)O)CCCCN.Cl.Cl
400 MHz in D2O
400 MHz in DMSO-d6
-
| 1H NMR |
399.65 MHz |
| C6 H14 N2 O2
|
saturated in D2O
|
| DL-lysine dihydrochloride
|
 |
Assign. Shift(ppm)
A 4.104
B 3.028
C 1.99
D 1.738
E 1.53
SOLVENT PEAK REMOVED
|
Hz ppm Int.
1646.48 4.120 536
1640.14 4.104 986
1636.60 4.096 106
1633.91 4.089 536
1223.88 3.063 41
1218.02 3.048 648
1210.33 3.029 990
1202.76 3.010 669
1198.12 2.998 44
833.98 2.087 89
828.13 2.073 164
823.24 2.060 137
822.39 2.058 150
819.46 2.051 259
817.38 2.046 235
815.92 2.042 106
813.72 2.037 437
811.40 2.031 184
808.84 2.024 345
807.98 2.022 328
802.86 2.009 689
799.80 2.002 99
798.95 2.000 113
796.63 1.994 560
793.82 1.987 106
791.99 1.982 283
789.92 1.977 324
788.21 1.973 181
786.25 1.968 338
785.52 1.966 341
781.62 1.956 171
779.66 1.951 304
777.71 1.946 150
777.47 1.946 150
775.51 1.941 116
771.85 1.932 137
771.00 1.930 143
765.14 1.915 113
710.69 1.779 246
702.88 1.759 775
695.07 1.740 1000
687.50 1.721 870
679.93 1.702 352
635.50 1.591 225
628.05 1.572 287
625.00 1.564 246
622.31 1.558 297
620.24 1.552 338
617.43 1.545 328
614.62 1.538 297
611.94 1.532 389
609.50 1.526 273
606.93 1.519 280
604.00 1.512 311
601.56 1.506 249
599.00 1.499 235
596.19 1.492 229
-
| 1H NMR |
399.65 MHz |
| C6 H14 N2 O2
|
0.038 g : 0.5 ml DMSO-d6
|
| DL-lysine dihydrochloride
|
|
Assign. Shift(ppm)
A *1 8.59
B *1 8.25
C 3.844
D 2.766
E 1.839
F 1.621
G *2 1.501
J *2 1.406
|
Hz ppm Int.
3433.53 8.592 996
3297.12 8.251 1000
1536.41 3.845 382
1098.02 2.748 589
746.15 1.868 307
738.53 1.848 746
731.66 1.831 788
724.18 1.813 390
663.15 1.660 154
655.82 1.641 466
648.35 1.623 675
640.87 1.604 561
633.54 1.586 260
617.37 1.545 158
610.05 1.527 218
603.64 1.511 293
596.31 1.493 306
588.84 1.474 179
572.66 1.433 201
565.19 1.415 281
558.32 1.398 258
551.61 1.381 205