2,2,3-三溴丁烷(62127-47-3)核磁图(¹³CNMR)

Mass

MS-KW-0552          
2,2,3-tribromobutane 
C4H7Br3             (Mass of molecular ion:    292)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       3.9
      27.0      27.2
      28.0       3.0
      29.0      10.2
      37.0       1.2
      38.0       2.3
      39.0      11.8
      43.0       1.1
      49.0       1.0
      50.0       4.3
      51.0       6.5
      52.0       2.4
      53.0      58.2
      54.0       5.8
      55.0      35.0
      56.0       1.8
      79.0       3.3
      80.0       5.3
      81.0       3.3
      82.0       5.2
      93.0       1.0
     105.0       3.3
     107.0       9.8
     109.0       6.4
     119.0       1.1
     133.0      26.4
     134.0       8.3
     135.0      26.3
     136.0       7.6
     137.0       1.0
     185.0       2.9
     187.0       5.7
     189.0       2.7
     213.0      51.6
     214.0       3.4
     215.0     100.0
     216.0       4.9
     217.0      48.4
     218.0       2.2

Assign. Shift(ppm) A 4.453 B 2.668 C 2.040

     Hz     ppm     Int.

   1789.80   4.477     72
   1783.33   4.461    205
   1776.74   4.445    208
   1770.27   4.429     76
   1066.53   2.668   1000
   1066.29   2.668    993
    818.73   2.048    666
    812.26   2.032    655