62439-33-2

丙基环己基苯甲酸对氰基苯酚酯(62439-33-2)质谱(MS)

产品名称:丙基环己基苯甲酸对氰基苯酚酯

CAS:62439-33-2

分子式:C17H21NO2

分子量: 271.35

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-4497          
p-cyanophenyl trans-4-propylcyclohexanecarboxylate
C17H21NO2           (Mass of molecular ion:    271)

   Source Temperature: 140 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      27.0       5.6
      29.0       6.4
      39.0       6.5
      40.0       1.1
      41.0      23.9
      42.0       2.0
      43.0       6.7
      53.0       3.8
      54.0       5.8
      55.0      29.3
      56.0       1.5
      57.0      16.0
      63.0       1.4
      64.0       1.8
      65.0       1.0
      67.0      11.8
      68.0       2.3
      69.0     100.0
      70.0       5.7
      71.0       1.0
      77.0       1.1
      79.0       2.3
      81.0      11.6
      82.0       3.9
      83.0      54.3
      84.0       3.7
      90.0       2.6
      91.0       1.0
      95.0       2.4
     102.0       1.8
     110.0       1.1
     119.0       2.8
     120.0       1.7
     123.0       1.3
     125.0      86.8
     126.0       9.0
     153.0      55.4
     154.0       6.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₇ H₂₁ N O₂	0.024 g : 0.5 ml CDCl₃
p-cyanophenyl trans-4-propylcyclohexanecarboxylate

    Assign.     Shift(ppm)

      A             7.678
      B             7.209
      C             2.491
      D             2.13
      E             1.88
      F             1.543
      G             1.33
      J             1.30
      K             1.21
      L             0.983
      M             0.895

     Hz     ppm     Int.

   3075.93   7.697     78
   3073.49   7.691    619
   3071.41   7.686    211
   3066.65   7.674    198
   3064.58   7.669    762
   3062.26   7.663    103
   2887.82   7.226     91
   2885.50   7.221    639
   2883.30   7.215    222
   2878.66   7.203    193
   2876.46   7.198    657
   2874.15   7.192     92
   1008.54   2.524     65
    999.88   2.502     65
    996.34   2.494    135
    992.68   2.484     74
    984.13   2.463     73
    858.03   2.147     94
    856.93   2.145     96
    856.45   2.144     95
    855.47   2.141    102
    854.61   2.139    106
    853.39   2.136     92
    851.07   2.130     51
    849.73   2.127     57
    848.27   2.123     49
    843.87   2.112    115
    843.14   2.110    110
    842.53   2.109    111
    841.19   2.105    119
    759.16   1.900    102
    758.79   1.899    100
    758.30   1.898     98
    758.06   1.897     98
    756.35   1.893    111
    755.98   1.892    113
    750.61   1.879     52
    750.00   1.877     51
    749.63   1.876     52
    747.92   1.872     64
    745.48   1.866    115
    743.77   1.862    104
    742.31   1.858    118
    739.14   1.850     54
    738.77   1.849     51
    637.57   1.596     49
    624.39   1.563    132
    620.73   1.554    125
    612.06   1.532    123
    608.40   1.523    126
    598.63   1.498     49
    546.02   1.367     71
    544.80   1.364     71
    538.70   1.348    124
    537.48   1.345    152
    534.55   1.338     70
    531.74   1.331    124
    530.27   1.327    197
    527.22   1.320     83
    525.63   1.316     58
    524.66   1.313     78
    523.07   1.309    148
    519.90   1.301     63
    518.19   1.297     55
    517.33   1.295     51
    515.99   1.292     72
    515.38   1.290     80
    511.72   1.281     54
    508.30   1.272     62
    490.97   1.229    141
    489.87   1.226    144
    485.72   1.216    124
    483.76   1.211    141
    482.54   1.208    148
    482.18   1.207    147
    481.20   1.205    138
    479.13   1.199     90
    476.68   1.193     82
    474.85   1.189    170
    469.36   1.175     51
    467.77   1.171     51
    412.84   1.034     60
    412.48   1.033     59
    409.55   1.025     61
    399.66   1.001    128
    396.00   0.991    117
    388.06   0.971     96
    386.47   0.968     88
    384.89   0.964    105
    382.93   0.959     73
    374.63   0.938     51
    371.34   0.930     64
    364.62   0.913    526
    360.60   0.903     50
    357.42   0.895   1000
    351.81   0.881     59
    350.22   0.877    411

in CDCl3