626-67-5

N-甲基哌啶(626-67-5)红外图谱(IR1)

产品名称:N-甲基哌啶

CAS:626-67-5

分子式:C6H13N

分子量: 99.17

InChI:InChI=1S/C6H13N/c1-7-5-3-2-4-6-7/h2-6H2,1H3

InChIKey: PAMIQIKDUOTOBW-UHFFFAOYSA-N

Smiles:N1(C)CCCCC1

Mass

MS-NW-3134          
1-methylpiperidine
C6H13N              (Mass of molecular ion:     99)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       4.1
      27.0       5.6
      28.0       2.8
      29.0       2.8
      30.0       1.9
      39.0       5.1
      41.0       7.3
      42.0      29.1
      43.0      46.4
      44.0       9.1
      53.0       1.3
      54.0       1.6
      55.0       6.0
      56.0       2.5
      57.0       8.6
      58.0      13.0
      68.0       1.6
      70.0      16.1
      71.0       9.5
      82.0       1.2
      84.0       7.7
      96.0       2.0
      98.0     100.0
      99.0      43.2
     100.0       2.7

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₁₃ N	0.05 ml : 0.5 ml CDCl₃
1-methylpiperidine

    Assign.     Shift(ppm)

      A             2.33
      B             2.234
      C             1.586
      D             1.41

     Hz     ppm     Int.

    929.69   2.327     94
    893.07   2.235   1000
    646.00   1.617    101
    640.14   1.602    239
    634.52   1.588    306
    628.78   1.574    284
    623.29   1.560    114
    563.23   1.410     73

¹H NMR	89.56 MHz
C₆ H₁₃ N	0.05 ml : 0.5 ml CDCl₃
1-methylpiperidine

    Assign.     Shift(ppm)

      A             2.33
      B             2.232
      C          1.59 to 1.48

     Hz     ppm     Int.

    213.38   2.383     53
    212.94   2.378     53
    208.88   2.333     89
    203.31   2.271     85
    200.00   2.234   1000
    197.31   2.204     32
    147.56   1.648     37
    143.06   1.598     58
    141.56   1.581     62
    137.06   1.531     62
    133.63   1.493     76
    133.06   1.486     73
    132.94   1.485     73
    130.00   1.452     40
    128.25   1.433     29
    126.06   1.408     22

in CDCl3