627-44-1

二乙基汞(627-44-1)质谱(MS)

产品名称:二乙基汞

CAS:627-44-1

分子式:C4H10Hg

分子量: 258.71

InChI:InChI=1S/2C2H5.Hg/c2*1-2;/h2*1H2,2H3;

InChIKey: SPIUPAOJDZNUJH-UHFFFAOYSA-N

Smiles:[Hg](CC)CC

Mass

MS-NW-3721          
diethylmercury
C4H10Hg             (Mass of molecular ion:    260)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      26.0       3.8
      27.0      21.4
      28.0       9.7
      29.0     100.0
      30.0       2.2
      41.0       1.2
      43.0       2.3
      58.0       1.8
     199.0       1.7
     200.0       2.4
     201.0       1.6
     202.0       3.0
     227.0       2.1
     228.0       3.6
     229.0       4.7
     230.0       3.3
     231.0       5.4
     233.0       1.2
     256.0       1.7
     257.0       3.0
     258.0       4.1
     259.0       2.5
     260.0       5.2
     262.0       1.1

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₄ H₁₀ Hg	0.05 ml : 0.5 ml CDCl₃
diethylmercury

    Assign.     Shift(ppm)

      A             1.289
      B             1.003
     
     SATELLITE PEAKS EXIST.

     Hz     ppm     Int.

    587.28   1.470     40
    579.35   1.450     72
    571.29   1.430     41
    542.97   1.359     31
    536.87   1.344     64
    535.03   1.339     45
    529.05   1.324    132
    528.56   1.323    146
    524.17   1.312    539
    520.87   1.304    118
    516.48   1.293    919
    515.99   1.292   1000
    508.18   1.272    596
    491.94   1.231     33
    451.54   1.130    182
    413.09   1.034    260
    405.27   1.015    618
    397.22   0.994    536
    388.92   0.974    157
    356.69   0.893     37
    348.63   0.873     34

¹H NMR	89.56 MHz
C₄ H₁₀ Hg	0.04 ml : 0.5 ml CDCl₃
diethylmercury

    Assign.     Shift(ppm)

      A             1.28
      B             0.99

     Hz     ppm     Int.

    186.75   2.086     31
    178.63   1.995     88
    170.88   1.908     39
    134.56   1.503     36
    128.19   1.432     31
    127.19   1.421     91
    124.38   1.389     80
    123.63   1.381    118
    121.81   1.361    119
    120.88   1.350    114
    118.19   1.320     89
    117.81   1.316     89
    115.31   1.288   1000
    113.63   1.269     37
    113.06   1.263     38
    112.31   1.255     32
    110.25   1.232    297
    109.44   1.222    352
    108.69   1.214    312
    107.94   1.206    346
     99.81   1.115    208
     98.00   1.095    170
     93.31   1.042    314
     92.75   1.036    289
     91.75   1.025    105
     86.13   0.962    140
     84.31   0.942    159
     80.19   0.896     42
     78.13   0.873     40
     74.69   0.834     30
     59.63   0.666     37
     52.00   0.581     82
     45.00   0.503     40
     43.75   0.489     31
     37.06   0.414     33

in CDCl3

liquid film

GAMMA-RAY IRRAD. IN SI(CH3)4 AT 77K, CENTRAL PART

ANION RADICAL, GAMMA-RAY IRRAD. IN SI(CH3)4 AT 77K

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