6299-67-8

2,3-二甲氧基苯胺(6299-67-8)质谱(MS)

产品名称:2,3-二甲氧基苯胺

CAS:6299-67-8

分子式:C8H11NO2

分子量: 153.18

InChI:InChI=1S/C8H11NO2/c1-10-7-5-3-4-6(9)8(7)11-2/h3-5H,9H2,1-2H3

InChIKey: HEZIOZBMPKPOER-UHFFFAOYSA-N

Smiles:C1(N)=CC=CC(OC)=C1OC

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-6145          
2,3-dimethoxyaniline
C8H11NO2            (Mass of molecular ion:    153)

   Source Temperature: 200 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.1
      28.0       3.2
      33.5       1.1
      38.0       1.5
      39.0       5.8
      40.0       1.2
      41.0       5.6
      50.0       1.2
      51.0       2.8
      52.0       4.7
      53.0       3.3
      54.0       1.0
      63.0       1.1
      65.0       7.5
      66.0       3.1
      67.0       9.9
      68.0       1.1
      76.5       1.1
      77.0       1.5
      78.0       1.9
      79.0       2.3
      80.0       5.3
      81.0       1.0
      82.0       1.5
      90.0       3.0
      92.0      10.9
      93.0      10.9
      94.0       2.7
      95.0      26.9
      96.0       2.1
     106.0       1.2
     107.0       1.2
     108.0      11.0
     109.0       3.3
     110.0      12.7
     111.0       1.2
     120.0       2.0
     137.0       2.2
     138.0     100.0
     139.0       8.3
     153.0      81.3
     154.0       7.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₁ N O₂	0.05 ml : 0.5 ml CDCl₃
2,3-dimethoxyaniline

    Assign.     Shift(ppm)

      A             6.819
      B             6.353
      C             6.313
      D     *1      3.806
      E     *1      3.799
      F             3.8

     Hz     ppm     Int.

   2734.01   6.842    138
   2725.83   6.821    261
   2717.65   6.801    162
   2543.70   6.365    158
   2542.36   6.362    184
   2535.64   6.345    153
   2534.30   6.342    167
   2527.83   6.326    143
   2526.49   6.322    122
   2519.65   6.305    130
   2518.19   6.301    115
   1521.12   3.807    939
   1518.43   3.800   1000

in CDCl3