三(2-甲基烯丙基)胺(6321-40-0)核磁图(¹³CNMR)

Mass

MS-IW-0865          
tris(2-methylallyl)amine
C12H21N             (Mass of molecular ion:    179)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.3
      29.0       7.1
      30.0       2.2
      39.0       3.5
      41.0       4.0
      42.0       4.4
      43.0       1.9
      44.0       1.2
      53.0       2.1
      55.0      32.2
      56.0       3.6
      58.0       1.0
      67.0       6.8
      68.0       2.0
      69.0       2.0
      70.0       2.3
      80.0       1.3
      81.0       3.1
      82.0       8.0
      83.0       1.1
      84.0       4.1
      94.0       1.5
      95.0       1.6
      96.0       2.7
     108.0       3.2
     109.0       2.8
     110.0       1.2
     111.0       1.0
     122.0       2.6
     123.0       5.6
     124.0       2.5
     136.0       7.7
     137.0       1.0
     138.0     100.0
     139.0      10.3
     164.0      12.4
     165.0       1.6
     178.0       1.3
     179.0      12.2
     180.0       1.8

Assign. Shift(ppm) A *1 4.899 B *1 4.822 C 2.784 D 1.734

     Hz     ppm     Int.

   1958.74   4.902    220
   1957.52   4.899    247
   1956.54   4.896    227
   1929.08   4.827    177
   1927.61   4.824    235
   1926.76   4.822    239
   1925.29   4.818    193
   1112.55   2.784    696
    693.36   1.735    866
    692.38   1.733   1000