6343-54-0

N-苄基甲酰胺(6343-54-0)红外图谱(IR1)

产品名称:N-苄基甲酰胺

CAS:6343-54-0

分子式:C8H9NO

分子量: 135.16

Mass

MS-IW-0762          
N-benzylformamide
C8H9NO              (Mass of molecular ion:    135)

   Source Temperature: 180 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      27.0       2.1
      28.0      10.9
      29.0       2.2
      30.0       4.7
      39.0       5.1
      41.0       3.3
      42.0       1.4
      43.0       3.1
      44.0       1.3
      50.0       2.9
      51.0       7.3
      52.0       2.2
      53.0       1.9
      55.0       2.5
      56.0       1.4
      57.0       4.6
      58.0       2.2
      63.0       2.9
      65.0       7.4
      70.0       2.1
      77.0      12.2
      78.0       5.7
      79.0      24.8
      80.0       2.1
      87.0       3.6
      89.0       5.6
      90.0       5.4
      91.0      30.8
      92.0       8.8
     104.0       3.3
     105.0       1.1
     106.0      24.2
     107.0       6.3
     108.0       1.1
     116.0       2.7
     117.0       1.7
     118.0       4.9
     134.0      43.9
     135.0     100.0
     136.0      10.5

400 MHz in CDCl3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₈ H₉ N O	0.05 ml : 0.5 ml CDCl₃
N-benzylformamide

    Assign.     Shift(ppm)

      A             8.465
      B             7.406
      C             7.268
      D             7.167
      E             3.305

     Hz     ppm     Int.

   3383.18   8.466    310
   2969.48   7.431     52
   2967.77   7.426    157
   2965.45   7.421     72
   2962.28   7.413     52
   2961.18   7.410    107
   2960.21   7.408    299
   2959.23   7.405    259
   2953.49   7.391    106
   2951.78   7.386    261
   2949.46   7.381     59
   2912.11   7.287     78
   2911.01   7.284    140
   2909.79   7.281     85
   2905.15   7.270     70
   2903.69   7.266    193
   2901.86   7.262     64
   2897.22   7.250     51
   2896.12   7.247     87
   2894.90   7.244     49
   2870.61   7.183     78
   2869.26   7.180    277
   2867.92   7.177    340
   2865.72   7.171     94
   2862.43   7.163    104
   2861.69   7.161    151
   2860.47   7.158    274
   2859.38   7.155    235
   2856.93   7.149     40
   1321.04   3.306   1000
   1320.43   3.304    908

¹H NMR	399.65 MHz
C₈ H₉ N O	0.036 g : 0.5 ml DMSO-d₆
N-benzylformamide

    Assign.     Shift(ppm)

      A             8.52
      B             8.150
      C             7.327
      D             7.27
      E             7.25
      F             4.311

     Hz     ppm     Int.

   3404.24   8.519     81
   3258.21   8.153    591
   3257.45   8.151    572
   3256.53   8.149    566
   2945.40   7.370     40
   2940.06   7.357     31
   2937.47   7.351    265
   2936.40   7.348    331
   2934.88   7.344    125
   2933.20   7.340     55
   2929.99   7.332    614
   2929.23   7.330    758
   2928.16   7.327    544
   2924.04   7.317    282
   2922.06   7.312    853
   2915.65   7.296     37
   2910.61   7.283    724
   2909.24   7.280   1000
   2908.78   7.279    976
   2906.49   7.273    234
   2902.07   7.262    682
   2901.46   7.261    588
   2897.95   7.252    215
   2895.81   7.246    427
   2893.22   7.240    112
   2890.17   7.232    106
   2888.64   7.228    157
   2887.12   7.225     81
   1726.23   4.320    989
   1719.97   4.304    985

in DMSO-d6