6358-20-9

5-(二乙氨基)-2-(亚硝基苯酚)(6358-20-9)质谱(MS)

产品名称:5-(二乙氨基)-2-(亚硝基苯酚)

CAS:6358-20-9

分子式:C10H14N2O2

分子量: 194.23

Mass

MS-NW-7457          
5-diethylamino-2-nitrosophenol
C10H14N2O2          (Mass of molecular ion:    194)

   Source Temperature: 170 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      15.0       1.3
      17.0       1.8
      18.0       7.8
      26.0       1.5
      27.0      10.3
      28.0       9.1
      29.0      13.9
      30.0       1.9
      38.0       2.1
      39.0       7.4
      40.0       1.9
      41.0       3.6
      42.0       6.2
      43.0       1.7
      44.0       2.9
      50.0       2.4
      51.0       6.0
      52.0       5.9
      53.0       6.8
      54.0       2.8
      55.0       2.6
      56.0       7.3
      58.0       2.7
      62.0       1.5
      63.0       4.5
      64.0       4.9
      65.0       7.3
      66.0       6.1
      67.0       2.8
      68.0       3.4
      69.0       1.0
      70.0       1.1
      72.0       2.7
      76.0       1.5
      77.0       4.6
      78.0       7.9
      79.0       9.4
      80.0       4.6
      81.0       2.3
      89.5       2.9
      90.0       1.0
      91.0       3.1
      92.0       7.7
      93.0       7.5
      94.0       5.2
      95.0       1.9
      97.0       1.6
     104.0       1.7
     105.0       1.7
     106.0       6.3
     107.0       5.3
     108.0       6.1
     109.0       1.9
     118.0       1.2
     119.0       3.0
     120.0       8.0
     121.0       7.0
     122.0       2.4
     123.0       1.2
     131.0       2.0
     132.0       1.5
     133.0       3.4
     134.0       3.8
     135.0       7.3
     136.0       8.9
     137.0       2.2
     147.0       1.7
     148.0       7.1
     149.0      82.8
     150.0      10.7
     151.0       1.8
     159.0       3.3
     162.0       1.2
     163.0       5.5
     164.0      16.6
     165.0       6.1
     166.0       1.4
     177.0      33.0
     178.0       5.1
     179.0      39.1
     180.0       5.8
     193.0       1.1
     194.0     100.0
     195.0      12.7
     196.0       1.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₄ N₂ O₂	0.033 g : 0.5 ml CDCl₃
5-diethylamino-2-nitrosophenol

    Assign.     Shift(ppm)

      A            18.51
      B             7.337
      C             6.572
      D             5.701
      E             3.511
      F             1.299

     Hz     ppm     Int.

   1657.99  18.513    272
    663.50   7.409    189
    653.61   7.299    314
    594.14   6.634    122
    591.61   6.606    120
    584.14   6.523     91
    581.61   6.495     92
    511.70   5.714    205
    509.17   5.686    185
    326.15   3.642    105
    318.89   3.561    369
    315.70   3.526     57
    315.26   3.521     57
    311.64   3.480    405
    307.90   3.438     50
    307.24   3.431     50
    306.91   3.427     51
    304.49   3.400    152
    123.45   1.379    488
    120.59   1.347     65
    116.30   1.299   1000
    109.04   1.218    432
    105.42   1.178     33
    104.98   1.173     31

in CDCl3