64063-37-2

2,6-二氯-3-甲基苯胺(64063-37-2)核磁图(¹HNMR)

产品名称:2,6-二氯-3-甲基苯胺

CAS:64063-37-2

分子式:C7H7Cl2N

分子量: 176.04

Mass

MS-NW-9911          
2,6-dichloro-3-methylaniline
C7H7Cl2N            (Mass of molecular ion:    175)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      37.0       1.0
      38.0       1.9
      39.0       2.9
      50.0       3.0
      50.5       1.2
      51.0       7.5
      51.5       8.7
      52.0       5.7
      52.5       1.8
      53.0       1.1
      61.0       1.1
      62.0       1.8
      63.0       1.9
      65.0       1.4
      69.5       4.9
      70.0       2.9
      70.5       1.7
      73.0       2.0
      74.0       2.3
      75.0       6.5
      76.0       3.5
      77.0      19.8
      78.0       4.5
      79.0       1.0
      85.0       1.1
      87.0       1.3
      87.5       2.6
      88.0       1.0
      88.5       1.6
     102.0       5.2
     103.0       1.2
     104.0      12.8
     105.0       4.6
     111.0      10.2
     112.0       6.6
     113.0      10.3
     114.0       2.1
     115.0       2.7
     123.0       1.4
     138.0       5.2
     139.0       3.1
     140.0     100.0
     141.0       9.1
     142.0      31.6
     143.0       2.7
     147.0       2.0
     149.0       1.3
     174.0      16.4
     175.0      89.7
     176.0      17.7
     177.0      57.3
     178.0       6.3
     179.0       9.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₇ H₇ Cl₂ N	0.036 g : 0.5 ml DMSO-d₆
2,6-dichloro-3-methylaniline

    Assign.     Shift(ppm)

      A             7.121
      B             6.571
      C             5.40
      D             2.249

     Hz     ppm     Int.

   2850.10   7.132    241
   2841.92   7.112    260
   2630.37   6.582    188
   2629.64   6.580    197
   2622.19   6.562    176
   2621.46   6.560    185
   2159.30   5.403    123
    898.68   2.249   1000

in DMSO-d6