64691-70-9

1,8-双(2-吡啶基)-3,6-二硫杂辛烷(64691-70-9)红外图谱(IR1)

产品名称:1,8-双(2-吡啶基)-3,6-二硫杂辛烷

CAS:64691-70-9

分子式:C16H20N2S2

分子量: 304.47

Mass

MS-NW-7936          
1,2-bis(2-(2-pyridyl)ethylthio)ethane
C16H20N2S2          (Mass of molecular ion:    304)

   Source Temperature: 180 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       1.9
      27.0       3.5
      28.0       2.0
      39.0       4.0
      45.0       2.8
      50.0       1.3
      51.0       6.7
      52.0       4.1
      53.0       3.3
      54.0       1.5
      59.0       1.3
      61.0       1.5
      65.0       4.4
      66.0       2.2
      77.0       4.2
      78.0      19.9
      79.0       7.6
      80.0       1.9
      92.0       4.6
      93.0      29.0
      94.0       5.9
     104.0       4.7
     105.0       3.3
     106.0      93.4
     107.0      11.1
     118.0       1.5
     132.0       2.1
     136.0       3.6
     137.0       1.6
     138.0      58.4
     139.0      43.9
     140.0       7.0
     141.0       2.2
     152.0       4.1
     166.0     100.0
     167.0      11.1
     168.0       5.2
     198.0       4.5
     199.0       3.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₆ H₂₀ N₂ S₂	0.047 g : 0.5 ml CDCl₃
1,2-bis(2-(2-pyridyl)ethylthio)ethane

    Assign.     Shift(ppm)

      A             8.538
      B             7.603
      C             7.177
      D             7.131
      E             3.059
      F             2.964
      G             2.716

     Hz     ppm     Int.

   3416.26   8.549     82
   3415.41   8.547     93
   3414.55   8.544     94
   3413.57   8.542     86
   3411.38   8.536     85
   3410.52   8.534     94
   3409.67   8.532     92
   3408.69   8.530     81
   3047.49   7.626     71
   3045.65   7.621     71
   3039.79   7.607    139
   3037.96   7.602    141
   3032.10   7.587     86
   3030.27   7.583     85
   2872.31   7.188    140
   2864.62   7.168    131
   2856.81   7.149     80
   2855.59   7.146     74
   2851.93   7.137     83
   2850.71   7.134     79
   2849.24   7.130     81
   2848.14   7.127     71
   2844.36   7.118     75
   2843.26   7.115     68
   1231.45   3.082     76
   1229.98   3.078     80
   1223.27   3.061    185
   1221.92   3.058    112
   1215.70   3.042    190
   1191.16   2.981    218
   1190.31   2.979    211
   1185.91   2.968     76
   1184.81   2.965    144
   1183.23   2.961    249
   1182.01   2.958    174
   1176.64   2.945    107
   1175.05   2.941     95
   1085.57   2.717   1000

in CDCl3