65119-95-1

22-二十三碳烯酸(65119-95-1)质谱(MS)

产品名称:22-二十三碳烯酸

CAS:65119-95-1

分子式:C23H44O2

分子量: 352.59

InChI:InChI=1S/C23H44O2/c1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20-21-22-23(24)25/h2H,1,3-22H2,(H,24,25)

InChIKey: YGTSVJQQDISEHZ-UHFFFAOYSA-N

Smiles:C(O)(=O)CCCCCCCCCCCCCCCCCCCCC=C

Mass

MS-NW-9379          
22-tricosenoic acid
C23H44O2            (Mass of molecular ion:    352)

   Source Temperature: 240 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      17.0       1.5
      18.0       7.5
      27.0       4.1
      28.0       2.5
      29.0      15.2
      39.0       5.3
      40.0       1.0
      41.0      52.7
      42.0      10.0
      43.0      59.4
      44.0       2.1
      45.0       3.1
      53.0       3.2
      54.0      10.7
      55.0     100.0
      56.0      30.2
      57.0      55.4
      58.0       2.7
      59.0       2.5
      60.0      14.1
      61.0       3.3
      66.0       1.3
      67.0      18.4
      68.0      15.9
      69.0      76.0
      70.0      30.2
      71.0      26.0
      72.0       1.5
      73.0      16.0
      74.0       1.5
      79.0       2.6
      80.0       3.4
      81.0      19.5
      82.0      26.2
      83.0      68.9
      84.0      30.8
      85.0      15.7
      86.0       1.2
      87.0       4.5
      93.0       2.4
      94.0       4.7
      95.0      15.0
      96.0      27.1
      97.0      64.3
      98.0      29.4
      99.0       6.5
     100.0       2.7
     101.0       5.5
     107.0       2.5
     108.0       3.6
     109.0       9.4
     110.0      14.7
     111.0      32.0
     112.0      12.0
     113.0       4.3
     114.0       6.0
     115.0       4.7
     116.0       1.5
     119.0       1.8
     121.0       4.3
     122.0       2.7
     123.0       8.2
     124.0       9.7
     125.0      17.4
     126.0       6.7
     127.0       6.8
     128.0       1.7
     129.0       5.1
     133.0       2.0
     134.0       3.5
     135.0       4.7
     136.0       2.1
     137.0       6.7
     138.0       7.8
     139.0      10.3
     140.0       4.5
     141.0       2.2
     143.0       2.4
     147.0       1.8
     148.0       3.3
     149.0       3.5
     150.0       1.5
     151.0       5.7
     152.0       7.0
     153.0       6.8
     154.0       3.3
     155.0       1.7
     157.0       1.8
     161.0       1.5
     162.0       1.1
     163.0       2.1
     164.0       1.0
     165.0       4.2
     166.0       4.4
     167.0       4.5
     168.0       2.3
     169.0       1.5
     171.0       1.6
     175.0       1.2
     177.0       1.3
     179.0       3.3
     180.0       3.2
     181.0       3.1
     182.0       1.8
     183.0       1.1
     185.0       1.6
     193.0       2.7
     194.0       3.2
     195.0       2.3
     196.0       1.4
     207.0       2.6
     208.0       3.7
     209.0       1.9
     210.0       1.2
     221.0       2.8
     222.0       3.7
     223.0       1.5
     224.0       1.0
     235.0       3.0
     236.0       4.2
     237.0       1.4
     249.0       3.2
     250.0       4.9
     251.0       1.4
     263.0       3.1
     264.0       3.0
     277.0       2.6
     278.0       2.2
     290.0       1.7
     291.0       2.5
     292.0       4.0
     293.0       1.0
     305.0       1.4
     306.0       1.3
     316.0       1.4
     334.0      18.1
     335.0       5.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₃ H₄₄ O₂	0.030 g : 0.5 ml CDCl₃
22-tricosenoic acid

    Assign.     Shift(ppm)

      A            11.
      B             5.811
      C             4.990
      D             4.925
      E             2.345
      F             2.038
      G             1.628
      J             1.37
      K             1.26
     
     J(B,C)=17.1HZ
     J(B,D)=10.3HZ
     J(B,F)=6.6HZ

     Hz     ppm     Int.

    944.91   2.365     36
    937.43   2.346     62
    929.74   2.327     39
    818.20   2.048     30
    500.88   1.254   1000

in CDCl3

KBr disc

nujol mull

TOKYO CHEMICAL INDUSTRY CO., LTD.

成都零六生物科技有限公司

九鼎化学（上海）科技有限公司

江苏艾康生物医药研发有限公司

Career Henan Chemica Co

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