6609-64-9

2-氯-2-氧-1,3,2-二氧磷杂环戊烷(6609-64-9)核磁图(¹HNMR)

产品名称:2-氯-2-氧-1,3,2-二氧磷杂环戊烷

CAS:6609-64-9

分子式:C2H4ClO3P

分子量: 142.48

InChI:InChI=1S/C2H4ClO3P/c3-7(4)5-1-2-6-7/h1-2H2

InChIKey: SBMUNILHNJLMBF-UHFFFAOYSA-N

Smiles:O1CCOP1(=O)Cl

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9240          
2-chloro-1,3,2-dioxaphospholane 2-oxide
C2H4ClO3P           (Mass of molecular ion:    142)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      14.0       1.1
      15.0       9.7
      26.0       2.9
      27.0      12.0
      28.0       7.8
      29.0      11.2
      30.0       3.7
      31.0      11.9
      36.0       3.0
      38.0       1.0
      42.0      36.6
      43.0      23.3
      44.0     100.0
      45.0       2.5
      47.0      29.7
      48.0      12.7
      49.0       2.9
      61.0       1.0
      62.0      16.2
      63.0       8.1
      64.0       5.8
      65.0       2.6
      66.0       1.2
      77.0      18.4
      78.0       2.0
      79.0       3.2
      81.0      35.1
      82.0       1.6
      83.0      32.6
      84.0       8.9
      85.0      10.7
      86.0       2.6
      91.0       1.4
      99.0       3.8
     100.0       5.1
     101.0       2.0
     102.0       1.5
     106.0       2.7
     107.0      84.0
     108.0       2.1
     112.0      87.0
     113.0       7.1
     114.0      34.2
     115.0       2.5
     116.0       2.8
     117.0       4.2
     119.0       2.6
     135.0       3.1
     137.0       2.1
     141.0       6.2
     142.0      22.6
     143.0       4.6
     144.0       7.5
     145.0       1.0
     147.0       5.9
     149.0       3.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂ H₄ Cl O₃ P	0.05 ml : 0.5 ml CDCl₃
2-chloro-1,3,2-dioxaphospholane 2-oxide

    Assign.     Shift(ppm)

      A     *1      4.624
      B     *1      4.545

     Hz     ppm     Int.

   1875.37   4.693     53
   1868.16   4.675    352
   1862.43   4.661    456
   1861.45   4.658    634
   1860.96   4.657    514
   1857.54   4.648    538
   1855.59   4.644    502
   1852.54   4.636    758
   1848.51   4.626    495
   1845.83   4.619    445
   1845.21   4.618    578
   1843.99   4.615    721
   1842.53   4.611    343
   1841.06   4.607    548
   1839.11   4.602    531
   1836.43   4.596    739
   1834.84   4.592    316
   1833.25   4.588    139
   1832.52   4.586    148
   1829.96   4.579    110
   1828.86   4.577    114
   1826.78   4.571    402
   1824.83   4.567    817
   1821.78   4.559    514
   1819.82   4.554    544
   1818.48   4.551    272
   1817.50   4.548    587
   1817.02   4.547    643
   1815.67   4.544   1000
   1812.99   4.537    512
   1810.91   4.532    532
   1809.94   4.529    269
   1809.20   4.527    515
   1807.98   4.524    674
   1806.76   4.521    483
   1806.15   4.520    380
   1804.08   4.515    137
   1802.00   4.509     73
   1800.05   4.505    293
   1793.82   4.489     43

in CDCl3