6935-27-9

2-苄氨基吡啶(6935-27-9)Raman光谱

产品名称:2-苄氨基吡啶

CAS:6935-27-9

分子式:C12H12N2

分子量: 184.24

InChI:InChI=1S/C12H12N2/c1-2-6-11(7-3-1)10-14-12-8-4-5-9-13-12/h1-9H,10H2,(H,13,14)

InChIKey: WYHXNQXDQQMTQI-UHFFFAOYSA-N

Smiles:C1(NCC2=CC=CC=C2)=NC=CC=C1

Mass

MS-NW-7014          
2-(benzylamino)pyridine
C12H12N2            (Mass of molecular ion:    184)

   Source Temperature: 160 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      17.0       1.2
      18.0       4.6
      27.0       2.4
      28.0       5.1
      38.0       2.0
      39.0       9.4
      40.0       1.5
      41.0       2.1
      50.0       2.9
      51.0      11.5
      52.0       8.9
      53.0       2.4
      62.0       1.0
      63.0       3.9
      64.0       1.7
      65.0      15.5
      66.0       2.0
      67.0       1.8
      76.0       1.2
      77.0       5.2
      78.0      24.5
      79.0      32.9
      80.0       8.2
      89.0       3.9
      90.0       1.7
      91.0      42.8
      92.0       5.5
     104.0       2.4
     105.0       3.7
     106.0      89.0
     107.0      20.4
     108.0       1.3
     127.0       1.2
     128.0       1.2
     154.0       2.7
     155.0       1.5
     156.0       2.7
     166.0       1.1
     167.0       1.9
     168.0       3.1
     169.0       1.0
     181.0       4.1
     182.0       2.7
     183.0      41.0
     184.0     100.0
     185.0      13.9
     186.0       1.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₂ N₂	0.041 g : 0.5 ml CDCl₃
2-(benzylamino)pyridine

    Assign.     Shift(ppm)

      A             8.064
      B             7.36
      C             7.34
      D             7.31
      E             7.251
      F             6.555
      G             6.341
      J             5.12
      K             4.480

     Hz     ppm     Int.

   3226.81   8.075    221
   3225.95   8.072    248
   3224.85   8.070    258
   3224.00   8.068    243
   3221.68   8.062    236
   3220.83   8.060    259
   3219.85   8.057    260
   3218.99   8.055    240
   2952.27   7.388    198
   2950.32   7.383    195
   2945.07   7.370    244
   2943.85   7.367    312
   2942.02   7.362    340
   2939.70   7.356    281
   2937.99   7.352    157
   2936.77   7.349    309
   2934.81   7.344    457
   2933.11   7.340    810
   2930.91   7.334   1000
   2930.05   7.332    897
   2927.86   7.327    199
   2926.51   7.323    107
   2923.95   7.317    571
   2923.10   7.315    849
   2921.26   7.310    325
   2917.24   7.300    189
   2916.02   7.297    247
   2915.28   7.295    293
   2905.27   7.270    178
   2903.44   7.265    254
   2902.10   7.262    110
   2901.49   7.261    147
   2899.41   7.255    122
   2896.61   7.248    257
   2890.50   7.233    140
   2890.01   7.232    136
   2626.46   6.572    287
   2625.61   6.570    297
   2621.46   6.560    295
   2620.48   6.557    320
   2619.38   6.555    307
   2618.41   6.552    302
   2615.97   6.546     40
   2614.26   6.542    276
   2613.40   6.540    284
   2539.18   6.354    283
   2538.33   6.352    493
   2537.35   6.349    294
   2530.76   6.333    280
   2529.91   6.331    484
   2528.93   6.328    289
   2046.88   5.122     96
   1793.33   4.488    816
   1787.48   4.473    791

in CDCl3