69770-20-3

3-(4-氯苯氧基)苯甲醛(69770-20-3)核磁图(¹³CNMR)

产品名称:3-(4-氯苯氧基)苯甲醛

CAS:69770-20-3

分子式:C13H9ClO2

分子量: 232.66

Mass

MS-IW-0555          
m-(p-chlorophenoxy)benzaldehyde
C13H9ClO2           (Mass of molecular ion:    232)

   Source Temperature: 260 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      38.0       1.3
      39.0       3.1
      44.0       1.1
      50.0       7.1
      51.0      13.5
      62.0       1.3
      63.0       5.2
      64.0       3.5
      65.0       2.3
      69.0       1.0
      69.5       4.4
      70.0       2.7
      73.0       2.1
      74.0       3.0
      75.0      12.0
      76.0       6.4
      77.0      13.3
      84.0       4.0
      85.0       1.2
      92.0       1.9
      98.0       2.5
      99.0       3.5
     101.0       1.3
     105.0       2.1
     111.0       4.6
     113.0       2.0
     115.0       4.5
     115.5       3.8
     116.0       1.0
     116.5       1.3
     127.0       1.4
     128.0       4.6
     130.0       1.4
     139.0       8.7
     140.0       4.1
     141.0      12.6
     142.0       1.6
     149.0       2.5
     151.0       1.1
     152.0       2.3
     153.0       1.2
     167.0       1.5
     168.0      38.2
     169.0      29.0
     170.0       3.6
     175.0       8.7
     176.0       2.5
     177.0       2.9
     179.0       1.1
     197.0       3.7
     198.0       1.2
     203.0      22.5
     204.0       4.9
     205.0       7.8
     206.0       1.5
     215.0      12.4
     216.0       2.0
     217.0       4.1
     231.0      33.3
     232.0     100.0
     233.0      24.5
     234.0      33.0
     235.0       4.6

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₉ Cl O₂	0.05 ml : 0.5 ml CDCl₃
m-(p-chlorophenoxy)benzaldehyde

    Assign.     Shift(ppm)

      A             9.943
      B             7.608
      C             7.503
      D             7.443
      E             7.310
      F             7.267
      G             6.964

     Hz     ppm     Int.

   3974.00   9.944   1000
   3046.42   7.623    131
   3045.35   7.621    209
   3043.98   7.617    133
   3038.94   7.605    192
   3037.72   7.601    290
   3036.35   7.598    175
   3006.29   7.523    226
   2998.50   7.503    335
   2990.72   7.484    187
   2976.84   7.449    241
   2975.31   7.445    251
   2974.24   7.443    278
   2972.72   7.439    237
   2929.38   7.330     66
   2926.03   7.322    773
   2923.74   7.316    215
   2919.31   7.305    239
   2917.18   7.300    746
   2913.67   7.291     84
   2909.70   7.281    182
   2908.63   7.278    186
   2907.41   7.275    234
   2906.04   7.272    160
   2901.61   7.261    155
   2900.54   7.258    146
   2899.02   7.254    144
   2897.95   7.252    130
   2790.68   6.983     78
   2787.48   6.975    809
   2785.19   6.970    220
   2780.61   6.958    208
   2778.47   6.953    637
   2775.12   6.944     63

in CDCl3