7260-11-9

3-羟基-2-萘甲酸苯酯(7260-11-9)核磁图(¹HNMR)

产品名称:3-羟基-2-萘甲酸苯酯

CAS:7260-11-9

分子式:C17H12O3

分子量: 264.28

Mass

MS-NW-8049          
phenyl 3-hydroxy-2-naphthoate
C17H12O3            (Mass of molecular ion:    264)

   Source Temperature: 180 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      39.0       3.2
      51.0       1.5
      62.0       1.0
      63.0       3.1
      65.0       3.0
      88.0       1.9
      89.0       3.7
     113.0       2.4
     114.0       6.0
     115.0      35.1
     116.0       3.5
     142.0       4.8
     143.0       3.6
     170.0       6.4
     171.0     100.0
     172.0      12.1
     173.0       1.0
     264.0      20.5
     265.0       3.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₇ H₁₂ O₃	0.040 g : 0.5 ml CDCl₃
phenyl 3-hydroxy-2-naphthoate

    Assign.     Shift(ppm)

      A            10.1
      B             8.717
      C             7.836
      D             7.692
      E             7.517
      F             7.466
      G             7.350
      J             7.34
      K             7.32
      L             7.258

     Hz     ppm     Int.

   4056.40  10.150   1000
   3484.19   8.719    677
   3136.44   7.848    229
   3135.68   7.847    246
   3128.05   7.827    256
   3127.29   7.826    267
   3078.61   7.704    233
   3070.98   7.685    286
   3070.22   7.683    292
   3012.39   7.538    171
   3011.02   7.535    181
   3005.52   7.521    218
   3004.15   7.517    295
   3002.78   7.514    155
   2997.13   7.500    181
   2995.91   7.497    178
   2994.84   7.494     77
   2992.55   7.488    291
   2990.57   7.483    141
   2987.52   7.476     73
   2986.30   7.473    164
   2985.08   7.470    532
   2984.47   7.468    512
   2982.03   7.462    108
   2978.67   7.454    185
   2976.84   7.449    469
   2974.40   7.443     83
   2941.13   7.360    211
   2939.91   7.357    235
   2937.62   7.351    692
   2935.18   7.345    195
   2933.96   7.342    419
   2932.89   7.339    468
   2931.67   7.336    233
   2928.16   7.327    134
   2926.48   7.323    427
   2924.80   7.319    287
   2920.23   7.307    102
   2919.01   7.304    176
   2917.94   7.302    109
   2906.65   7.273    115
   2905.27   7.270    549
   2904.21   7.267    660
   2901.92   7.262    177
   2898.56   7.253    177
   2897.80   7.251    282
   2896.73   7.249    514
   2895.51   7.246    472
   2893.07   7.240     64

in CDCl3