7355-51-3

4-(2-环己烯氧基)苯甲酸(7355-51-3)核磁图(¹HNMR)

产品名称:4-(2-环己烯氧基)苯甲酸

CAS:7355-51-3

分子式:C13H14O3

分子量: 218.25

Mass

MS-NW-7764          
p-(2-cyclohexenyloxy)benzoic acid
C13H14O3            (Mass of molecular ion:    218)

   Source Temperature: 180 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      27.0      10.3
      28.0       1.0
      29.0       2.2
      38.0       3.6
      39.0      15.7
      40.0       1.7
      41.0      13.2
      45.0       1.4
      50.0       3.7
      51.0       6.2
      52.0       3.5
      53.0      18.5
      54.0       1.8
      55.0       3.3
      62.0       1.9
      63.0       6.8
      64.0       3.6
      65.0      11.4
      66.0       3.3
      75.0       1.2
      76.0       1.4
      77.0       9.9
      78.0       2.3
      79.0      33.6
      80.0      77.0
      81.0     100.0
      82.0       6.5
      91.0       1.0
      92.0       2.1
      93.0       2.4
      95.0       1.7
     109.0       2.1
     121.0       8.8
     137.0       1.0
     138.0       3.7
     139.0      16.8
     140.0       1.4
     218.0       4.9

400 MHz at 60C

¹H NMR	399.65 MHz
C₁₃ H₁₄ O₃	0.039 g : 0.5 ml CDCl₃ at 60C
p-(2-cyclohexenyloxy)benzoic acid

    Assign.     Shift(ppm)

      A            11.
      B             8.041
      C             6.942
      D             5.981
      E             5.853
      F             4.874
      G     *1      2.128
      J     *1      2.03
      K     *2      1.97
      L             1.89
      M     *2      1.658

     Hz     ppm     Int.

   3221.35   8.061    131
   3218.42   8.054    902
   3216.40   8.049    300
   3214.21   8.043     69
   3211.64   8.037    297
   3209.44   8.031   1000
   3206.70   8.024    114
   2781.75   6.961    126
   2778.82   6.954    843
   2776.99   6.949    275
   2772.04   6.937    256
   2770.03   6.932    818
   2767.10   6.924     92
   2400.40   6.007     75
   2399.30   6.004     82
   2396.73   5.998    134
   2395.63   5.995    140
   2393.07   5.988     83
   2391.97   5.986     86
   2390.32   5.982    110
   2389.22   5.979    113
   2386.66   5.972    185
   2385.56   5.970    195
   2383.00   5.963    106
   2381.90   5.960    102
   2347.10   5.873     93
   2344.90   5.868    177
   2341.78   5.860    178
   2339.59   5.855     89
   2337.02   5.848     65
   2334.82   5.843    120
   2331.71   5.835    120
   2329.51   5.829     60
   1955.12   4.893     64
   1953.84   4.889     85
   1952.01   4.885    110
   1950.36   4.881    137
   1949.07   4.877    148
   1948.16   4.875    144
   1946.88   4.872    146
   1945.04   4.867    133
   1943.40   4.863    104
   1941.38   4.858     74
   1940.10   4.855     55

in CDCl3