N-(2-氯乙基)乙酰胺(7355-58-0)核磁图(¹³CNMR)

Mass

MS-KW-0163          
N-(2-chloroethyl)acetamide
C4H8ClNO            (Mass of molecular ion:    121)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      14.0       2.5
      15.0      14.5
      18.0       2.1
      26.0       3.8
      27.0      13.9
      28.0      19.8
      29.0       4.6
      30.0     100.0
      31.0       1.7
      35.0       1.1
      36.0      12.3
      38.0       4.4
      40.0       2.9
      41.0       4.6
      42.0      18.6
      43.0      90.5
      44.0      30.7
      45.0       3.2
      49.0       2.0
      51.0       1.1
      52.0       1.4
      54.0      20.6
      55.0      84.3
      56.0       9.1
      59.0       2.4
      60.0       4.0
      63.0      10.5
      65.0       3.3
      72.0      62.9
      73.0       3.2
      78.0       3.8
      80.0       1.7
      84.0       1.8
      85.0      57.6
      86.0      11.7
     106.0       2.6
     121.0      20.7
     122.0       2.0
     123.0       6.6

Assign. Shift(ppm) A 7.77 B 3.628 C 3.577 D 2.072

     Hz     ppm     Int.

   3106.20   7.773     41
   1458.62   3.650     94
   1456.67   3.645    107
   1453.37   3.637    110
   1450.93   3.631    338
   1446.41   3.620    253
   1445.43   3.617    262
   1437.50   3.597    125
   1436.89   3.596    126
   1432.25   3.584    217
   1426.51   3.570    155
   1424.56   3.565     90
   1420.65   3.555     46
   1419.07   3.551     41
    832.76   2.084     63
    828.37   2.073   1000