73592-81-1

1-氰基-4-(反-4-乙基环己基)苯(73592-81-1)质谱(MS)

产品名称:1-氰基-4-(反-4-乙基环己基)苯

CAS:73592-81-1

分子式:C15H19N

分子量: 213.32

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-4508          
p-(4-ethylcyclohexyl)benzonitrile
C15H19N             (Mass of molecular ion:    213)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      18.0       1.1
      27.0      12.7
      28.0       1.4
      29.0      15.8
      39.0      16.8
      40.0       2.3
      41.0      39.4
      42.0       6.7
      43.0      26.7
      50.0       2.5
      51.0       5.4
      52.0       2.3
      53.0       6.1
      54.0       7.3
      55.0      50.3
      56.0      11.6
      57.0       1.1
      62.0       1.3
      63.0       4.1
      64.0       1.8
      65.0       2.9
      66.0       1.7
      67.0      15.4
      68.0       5.9
      69.0      29.7
      70.0       7.3
      71.0      12.0
      74.0       1.0
      75.0       2.7
      76.0       3.6
      77.0       6.7
      78.0       2.9
      79.0       2.9
      80.0       2.7
      81.0      47.0
      82.0      12.0
      83.0       4.2
      84.0      50.1
      85.0       3.4
      88.0       1.2
      89.0       9.6
      90.0       3.1
      91.0       2.0
      95.0      14.5
      96.0       3.0
      97.0       9.6
     101.0       3.5
     102.0       7.5
     103.0       8.9
     104.0      10.7
     105.0       1.3
     107.0       3.2
     108.0      23.7
     109.0       7.2
     110.0      20.5
     111.0       1.9
     113.0       1.2
     114.0       2.0
     115.0      13.2
     116.0      76.1
     117.0      24.1
     118.0       3.0
     127.0       4.0
     128.0      10.3
     129.0     100.0
     130.0      53.8
     131.0      10.8
     132.0       1.1
     140.0       8.0
     141.0       3.5
     142.0      44.9
     143.0      47.3
     144.0      13.0
     145.0      11.2
     146.0       1.4
     153.0       1.7
     154.0       3.1
     155.0       2.5
     156.0       6.7
     157.0       5.6
     158.0       2.8
     159.0       2.3
     167.0       4.0
     168.0       2.1
     170.0       3.3
     171.0       1.0
     172.0       1.0
     182.0       1.1
     183.0       1.6
     184.0      19.2
     185.0       6.4
     186.0       1.0
     198.0       2.1
     212.0       3.2
     213.0      88.8
     214.0      15.6
     215.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₅ H₁₉ N	0.033 g : 0.5 ml CDCl₃
p-(4-ethylcyclohexyl)benzonitrile

    Assign.     Shift(ppm)

      A             7.565
      B             7.301
      C             2.521
      D             1.89
      E             1.432
      F             1.270
      G             1.20
      J             1.053
      K             0.911

     Hz     ppm     Int.

   3029.79   7.582     84
   3028.08   7.577    472
   3026.25   7.573    176
   3021.48   7.561    187
   3019.65   7.556    569
   3017.94   7.552    103
   2923.83   7.316     84
   2923.34   7.315     94
   2922.12   7.312    408
   2921.63   7.311    535
   2920.17   7.307    163
   2919.68   7.306    146
   2917.85   7.302     37
   2917.60   7.301     37
   2917.24   7.300     36
   2915.04   7.294    150
   2913.57   7.291    461
   2913.09   7.290    352
   2911.87   7.287     82
   2903.93   7.267    613
   1020.02   2.553     51
   1016.72   2.545     33
   1010.86   2.530     56
   1007.81   2.522    104
   1004.52   2.514     60
    998.66   2.499     33
    995.61   2.492     55
    766.72   1.919    119
    763.43   1.911    168
    760.25   1.903    222
    757.57   1.896    164
    755.62   1.891    137
    752.56   1.884    177
    750.37   1.878    218
    748.78   1.874    187
    747.31   1.870    166
    744.02   1.862    119
    740.72   1.854     44
    593.99   1.487     38
    589.97   1.477     52
    580.32   1.453    121
    577.15   1.445    114
    567.99   1.422    134
    564.94   1.414    118
    555.18   1.390     49
    552.25   1.382     48
    523.68   1.311     40
    522.46   1.308     39
    516.48   1.293    154
    515.01   1.289    104
    509.16   1.275    297
    502.08   1.257    251
    495.36   1.240     85
    494.26   1.237     84
    491.09   1.229     44
    488.04   1.222     58
    484.99   1.214     40
    482.54   1.208     45
    480.71   1.203     43
    479.86   1.201     46
    478.15   1.197     34
    476.68   1.193     46
    475.34   1.190     34
    473.75   1.186     39
    470.83   1.179     37
    469.73   1.176     35
    438.60   1.098     70
    435.55   1.090     70
    425.90   1.066    125
    422.73   1.058    126
    412.72   1.033     96
    409.06   1.024     55
    401.61   1.005     40
    374.88   0.939     37
    370.85   0.928    531
    363.65   0.910   1000
    359.86   0.901     37
    356.20   0.892    440

in CDCl3