2-羟甲基-15-冠-5(75507-25-4)核磁图(¹HNMR)

Mass

MS2001-00884WA      
2-(hydroxymethyl)-15-crown 5-ether
C11H22O6            (Mass of molecular ion:    250)

   Source Temperature: 235 °C
   Sample Temperature: 300 °C
   Reservoir, 70 eV

      15.0       3.7
      18.0       1.8
      19.0       1.8
      26.0       1.1
      27.0       7.8
      28.0       6.1
      29.0       9.4
      30.0       2.3
      31.0      23.7
      32.0       1.0
      39.0       1.1
      41.0       7.9
      42.0       6.3
      43.0      41.5
      44.0      20.6
      45.0     100.0
      46.0       2.9
      55.0       1.6
      56.0       2.1
      57.0      19.5
      58.0      19.0
      59.0      31.3
      60.0       1.4
      61.0       2.7
      69.0       4.2
      70.0       4.5
      71.0       7.2
      72.0      12.2
      73.0      27.7
      74.0       5.6
      75.0      11.5
      83.0       1.1
      84.0       1.0
      85.0       1.2
      86.0       8.6
      87.0      80.8
      88.0      19.9
      89.0      41.0
      90.0       2.7
      99.0       3.3
     100.0       6.2
     101.0      11.9
     102.0       3.5
     103.0       6.6
     104.0       1.1
     105.0       1.3
     107.0       1.4
     113.0       3.2
     114.0       1.4
     115.0       2.6
     116.0       2.3
     117.0       5.3
     118.0       2.4
     119.0       6.1
     131.0      12.7
     132.0       1.5
     133.0      15.6
     134.0       1.2
     135.0       1.9
     144.0       1.2
     145.0       3.1
     147.0       1.1
     161.0       2.7
     163.0       3.1
     175.0       1.3
     177.0       2.6
     207.0       1.2
     219.0      21.0
     220.0       2.5