75568-11-5

3,5-二溴邻苯二胺单盐酸盐(75568-11-5)质谱(MS)

产品名称:3,5-二溴邻苯二胺单盐酸盐

CAS:75568-11-5

分子式:C6H7Br2ClN2

分子量: 302.39

¹HNMR

IR1

IR2

Mass

MS-NW-9953          
3,5-dibromo-o-phenylenediamine monohydrochloride
C6H6Br2N2 HCl       (Mass of molecular ion:    264)

   Source Temperature: 140 °C
   Sample Temperature:  90 °C
   Direct, 75 eV

      17.0       2.7
      18.0      14.8
      28.0       4.7
      35.0       1.9
      36.0      25.1
      37.0       1.2
      38.0       8.4
      50.0       3.2
      51.0       5.7
      52.0       9.4
      52.5       2.8
      53.0       9.1
      54.0       1.3
      61.0       1.0
      62.0       1.9
      63.0       1.0
      65.0       1.3
      75.0       1.2
      76.0       4.6
      77.0       2.3
      78.0      10.3
      79.0       4.8
      80.0       1.6
      82.0       1.4
      89.0       1.8
      92.0       1.5
      92.5       1.2
      93.0       1.7
      93.5       1.2
     103.0       1.0
     105.0      10.5
     106.0      13.0
     107.0       1.0
     132.0       2.4
     133.0       4.4
     134.0       2.0
     156.0       1.1
     157.0       1.2
     158.0       6.7
     159.0       1.5
     160.0       5.6
     168.0       2.4
     170.0       2.4
     183.0       1.0
     184.0       2.4
     185.0      10.9
     186.0       3.5
     187.0       9.7
     188.0       1.1
     236.0       1.8
     238.0       3.5
     240.0       1.7
     263.0       1.9
     264.0      51.2
     265.0       7.4
     266.0     100.0
     267.0       9.2
     268.0      48.7
     269.0       3.6

parameter in DMSO-d6

¹H NMR	300 MHz
C₆ H₆ Br₂ N₂	0.032 g : 0.5 ml DMSO-d₆
3,5-dibromo-o-phenylenediamine monohydrochloride

    Parameter     ppm  Hz

      D(A)         7.494
      D(B)         7.352
       J(A,B)          2.2
     
      D(C)         6.2

     Hz     ppm     Int.

   2249.33   7.498    911
   2247.14   7.490   1000
   2206.67   7.356   1000
   2204.48   7.348    911
   1859.98   6.200     73

KBr disc

nujol mull