7623-13-4

2,3-二氯丙酰氯(7623-13-4)核磁图(¹³CNMR)

产品名称:2,3-二氯丙酰氯

CAS:7623-13-4

分子式:C3H3Cl3O

分子量: 161.41

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-7461          
2,3-dichloropropionyl chloride
C3H3Cl3O            (Mass of molecular ion:    160)

   Source Temperature: 250 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      18.0       1.0
      24.0       1.2
      25.0       6.4
      26.0      23.2
      27.0      26.2
      28.0       5.3
      29.0       1.3
      35.0       5.6
      36.0      10.4
      37.0       2.1
      38.0       3.3
      42.0       1.1
      44.0       2.0
      45.0       1.1
      47.0       2.4
      48.0       3.4
      49.0       6.6
      50.0       1.2
      51.0       2.4
      53.0       2.8
      54.0       1.0
      55.0      10.7
      60.0       4.2
      61.0      72.6
      62.0      70.4
      63.0      39.1
      64.0      22.1
      65.0       6.5
      76.0       5.1
      78.0       1.8
      83.0       2.1
      85.0       1.5
      89.0      23.1
      90.0       1.0
      91.0       7.7
      96.0       4.2
      97.0     100.0
      98.0       4.8
      99.0      61.7
     100.0       1.9
     101.0      10.2
     107.0       1.0
     124.0       1.5
     125.0      42.2
     126.0       2.7
     127.0      25.8
     128.0       1.2
     129.0       4.7

parameter in CDCl3

¹H NMR	300 MHz
C₃ H₃ Cl₃ O	0.05 ml : 0.5 ml CDCl₃
2,3-dichloropropionyl chloride

    Parameter     ppm  Hz

      D(A)         4.769
      D(B)  *1     3.994
      D(C)  *1     3.962
       J(A,B)          7.7
       J(A,C)          5.1
       J(B,C)        -11.7

     Hz     ppm     Int.

   1437.19   4.791    520
   1431.55   4.772    573
   1430.04   4.767    581
   1424.40   4.748    579
   1210.35   4.034    156
   1203.20   4.011    105
   1198.65   3.995    983
   1194.45   3.981    994
   1191.50   3.972   1000
   1188.82   3.963    991
   1182.76   3.943    156
   1177.12   3.924    101

in CDCl3