77-57-6

1-苯基-1-氰基环戊烷(77-57-6)质谱(MS)

产品名称:1-苯基-1-氰基环戊烷

CAS:77-57-6

分子式:C12H13N

分子量: 171.24

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-1256          
1-phenyl-1-cyclopentanecarbonitrile
C12H13N             (Mass of molecular ion:    171)

   Source Temperature: 230 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      27.0       1.0
      39.0       2.9
      41.0       2.3
      50.0       1.0
      51.0       3.1
      55.0       1.1
      63.0       1.5
      65.0       1.5
      76.0       1.2
      77.0       3.5
      78.0       3.2
      89.0       1.7
      91.0       2.9
     102.0       6.3
     103.0       5.6
     104.0       1.0
     115.0       8.4
     116.0       4.1
     117.0       4.4
     118.0       1.0
     128.0       5.5
     129.0     100.0
     130.0      14.1
     131.0       1.2
     140.0       1.3
     142.0       4.0
     143.0      13.0
     144.0       5.1
     156.0       1.4
     170.0       6.8
     171.0      28.0
     172.0       3.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₃ N	0.05 ml : 0.5 ml CDCl₃
1-phenyl-1-cyclopentanecarbonitrile

    Assign.     Shift(ppm)

      A             7.439
      B             7.353
      C             7.281
      D             2.439
      E             2.02
      F             1.908

     Hz     ppm     Int.

   2979.25   7.455    511
   2977.78   7.451    750
   2975.71   7.446    234
   2971.92   7.437    466
   2970.58   7.433    842
   2969.60   7.431    894
   2967.16   7.425    172
   2947.63   7.376    144
   2946.66   7.374    329
   2945.68   7.371    541
   2943.73   7.366    203
   2940.80   7.359    170
   2938.48   7.353   1000
   2936.89   7.349    508
   2932.37   7.338    278
   2930.66   7.334    577
   2928.47   7.328    117
   2916.87   7.299    257
   2915.53   7.296    481
   2914.18   7.292    273
   2912.11   7.287     33
   2911.87   7.287     33
   2910.40   7.283    175
   2908.20   7.277    527
   2905.88   7.272    146
   2902.22   7.262    112
   2901.00   7.259    200
   2899.66   7.256    111
    976.07   2.443    282
    968.75   2.424    280
    826.90   2.070    294
    814.09   2.038    370
    812.50   2.034    311
    811.40   2.031    302
    810.30   2.028    405
    808.72   2.024    626
    806.76   2.019    333
    805.42   2.016    295
    768.43   1.923    300
    762.33   1.908    332

in CDCl3