4-苯基哌啶(771-99-3)核磁图(13CNMR)
InChI:InChI=1S/C11H15N/c1-2-4-10(5-3-1)11-6-8-12-9-7-11/h1-5,11-12H,6-9H2
InChIKey: UTBULQCHEUWJNV-UHFFFAOYSA-N
Smiles:N1CCC(C2=CC=CC=C2)CC1
-
Mass
MS-NW-6792
4-phenylpiperidine
C11H15N (Mass of molecular ion: 161)
Source Temperature: 260 °C
Sample Temperature: 190 °C
Reservoir, 75 eV
15.0 1.3
18.0 2.2
27.0 5.0
28.0 21.5
29.0 20.6
30.0 42.5
39.0 5.6
41.0 3.5
42.0 16.4
43.0 56.8
44.0 31.9
50.0 1.4
51.0 6.5
52.0 2.4
53.0 2.8
54.0 2.4
55.0 5.7
56.0 100.0
57.0 72.4
58.0 3.0
63.0 2.4
65.0 4.6
68.0 5.3
69.0 7.7
70.0 2.7
76.0 1.3
77.0 10.1
78.0 7.8
79.0 2.1
80.0 1.3
80.5 1.2
82.0 5.9
83.0 24.2
84.0 2.7
89.0 1.8
91.0 14.7
92.0 1.7
102.0 2.7
103.0 8.2
104.0 14.3
105.0 5.3
106.0 1.8
115.0 7.4
116.0 2.9
117.0 6.7
118.0 5.8
119.0 1.9
120.0 1.6
127.0 1.4
128.0 2.6
129.0 3.3
130.0 3.1
131.0 2.5
132.0 3.5
133.0 1.3
143.0 1.0
144.0 1.5
145.5 1.7
154.0 1.0
155.0 4.0
158.0 1.0
159.0 2.4
160.0 34.9
161.0 84.8
162.0 10.7
90 MHz in CDCl3
400 MHz in CDCl3
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| 1H NMR |
89.56 MHz |
| C11 H15 N
|
0.039 g : 0.5 ml CDCl3
|
| 4-phenylpiperidine
|
 |
Assign. Shift(ppm)
A 7.31 to 7.15
B 3.155
C 2.72
D 2.61
E 1.86
F 1.89 to 1.75
G 1.60
400MHZ : HSP-41-831
|
Hz ppm Int.
661.19 7.383 46
657.50 7.342 33
655.81 7.323 56
653.81 7.301 97
652.94 7.291 115
651.56 7.276 169
648.63 7.243 1000
647.69 7.232 979
644.44 7.196 176
643.06 7.181 70
642.31 7.172 68
641.75 7.166 65
640.13 7.148 92
294.25 3.286 36
293.69 3.280 39
290.56 3.245 65
287.88 3.215 52
281.81 3.147 73
281.50 3.144 74
278.75 3.113 123
278.31 3.108 122
276.19 3.084 85
275.75 3.079 84
256.88 2.869 96
253.31 2.829 80
245.56 2.742 144
242.38 2.707 138
237.94 2.657 51
233.75 2.610 146
230.06 2.569 95
226.69 2.532 43
222.50 2.485 70
218.06 2.435 42
173.13 1.934 36
172.44 1.926 37
166.88 1.864 232
163.00 1.821 165
162.31 1.813 168
160.25 1.790 171
159.00 1.776 192
158.63 1.772 192
156.44 1.747 140
154.94 1.731 79
153.75 1.717 67
151.94 1.697 134
147.81 1.651 138
140.38 1.568 54
138.75 1.550 43
136.25 1.522 57
134.81 1.506 42
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| 1H NMR |
399.65 MHz |
| C11 H15 N
|
0.034 g : 0.5 ml CDCl3
|
| 4-phenylpiperidine
|
|
Assign. Shift(ppm)
A 7.296
B 7.22
C 7.19
D 3.178
E 2.734
F 2.606
G 1.97
J 1.823
K 1.642
90MHZ : HSP-03-779
|
Hz ppm Int.
2925.42 7.320 233
2924.56 7.318 370
2922.97 7.314 183
2917.85 7.302 611
2917.11 7.300 780
2913.57 7.291 97
2911.62 7.286 296
2909.79 7.281 755
2908.08 7.277 238
2904.42 7.268 53
2902.83 7.264 48
2901.86 7.262 49
2901.00 7.259 50
2900.02 7.257 50
2898.93 7.254 52
2898.32 7.253 53
2890.14 7.232 622
2888.79 7.229 1000
2886.96 7.224 292
2881.59 7.211 797
2880.86 7.209 645
2880.37 7.208 669
2878.78 7.204 271
2874.88 7.194 231
2872.92 7.189 498
2870.85 7.184 161
2867.19 7.175 145
2865.84 7.171 221
2864.38 7.168 121
1276.00 3.193 271
1264.04 3.163 304
1105.59 2.767 218
1103.15 2.761 229
1098.88 2.750 61
1093.38 2.736 405
1091.06 2.731 407
1085.69 2.717 54
1085.08 2.716 55
1081.18 2.706 210
1078.86 2.700 199
1057.37 2.646 68
1053.71 2.637 121
1049.93 2.628 75
1047.85 2.622 36
1045.29 2.616 136
1041.63 2.607 245
1037.96 2.598 138
1033.20 2.586 80
1029.54 2.577 135
1025.88 2.567 74
787.96 1.972 151
736.08 1.842 265
722.17 1.808 354
675.05 1.690 168
671.02 1.680 170
667.36 1.670 43
662.96 1.659 345
661.99 1.657 306
658.81 1.649 371
650.76 1.629 244
649.66 1.626 308
646.61 1.618 267
645.63 1.616 271
637.45 1.596 108
633.42 1.585 104