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771-99-3

4-苯基哌啶(771-99-3)核磁图(13CNMR)

产品名称:4-苯基哌啶

CAS:771-99-3

分子式:C11H15N

分子量: 161.24

InChI:InChI=1S/C11H15N/c1-2-4-10(5-3-1)11-6-8-12-9-7-11/h1-5,11-12H,6-9H2

InChIKey: UTBULQCHEUWJNV-UHFFFAOYSA-N

Smiles:N1CCC(C2=CC=CC=C2)CC1

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    Mass

    MS-NW-6792          
    4-phenylpiperidine
    C11H15N             (Mass of molecular ion:    161)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       1.3
          18.0       2.2
          27.0       5.0
          28.0      21.5
          29.0      20.6
          30.0      42.5
          39.0       5.6
          41.0       3.5
          42.0      16.4
          43.0      56.8
          44.0      31.9
          50.0       1.4
          51.0       6.5
          52.0       2.4
          53.0       2.8
          54.0       2.4
          55.0       5.7
          56.0     100.0
          57.0      72.4
          58.0       3.0
          63.0       2.4
          65.0       4.6
          68.0       5.3
          69.0       7.7
          70.0       2.7
          76.0       1.3
          77.0      10.1
          78.0       7.8
          79.0       2.1
          80.0       1.3
          80.5       1.2
          82.0       5.9
          83.0      24.2
          84.0       2.7
          89.0       1.8
          91.0      14.7
          92.0       1.7
         102.0       2.7
         103.0       8.2
         104.0      14.3
         105.0       5.3
         106.0       1.8
         115.0       7.4
         116.0       2.9
         117.0       6.7
         118.0       5.8
         119.0       1.9
         120.0       1.6
         127.0       1.4
         128.0       2.6
         129.0       3.3
         130.0       3.1
         131.0       2.5
         132.0       3.5
         133.0       1.3
         143.0       1.0
         144.0       1.5
         145.5       1.7
         154.0       1.0
         155.0       4.0
         158.0       1.0
         159.0       2.4
         160.0      34.9
         161.0      84.8
         162.0      10.7
    

90 MHz in CDCl3

400 MHz in CDCl3

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    1H NMR 89.56 MHz
    C11 H15 N 0.039 g : 0.5 ml CDCl3
    4-phenylpiperidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.31 to 7.15 B 3.155 C 2.72 D 2.61 E 1.86 F 1.89 to 1.75 G 1.60 400MHZ : HSP-41-831

         Hz     ppm     Int.
    

        661.19   7.383     46
        657.50   7.342     33
        655.81   7.323     56
        653.81   7.301     97
        652.94   7.291    115
        651.56   7.276    169
        648.63   7.243   1000
        647.69   7.232    979
        644.44   7.196    176
        643.06   7.181     70
        642.31   7.172     68
        641.75   7.166     65
        640.13   7.148     92
        294.25   3.286     36
        293.69   3.280     39
        290.56   3.245     65
        287.88   3.215     52
        281.81   3.147     73
        281.50   3.144     74
        278.75   3.113    123
        278.31   3.108    122
        276.19   3.084     85
        275.75   3.079     84
        256.88   2.869     96
        253.31   2.829     80
        245.56   2.742    144
        242.38   2.707    138
        237.94   2.657     51
        233.75   2.610    146
        230.06   2.569     95
        226.69   2.532     43
        222.50   2.485     70
        218.06   2.435     42
        173.13   1.934     36
        172.44   1.926     37
        166.88   1.864    232
        163.00   1.821    165
        162.31   1.813    168
        160.25   1.790    171
        159.00   1.776    192
        158.63   1.772    192
        156.44   1.747    140
        154.94   1.731     79
        153.75   1.717     67
        151.94   1.697    134
        147.81   1.651    138
        140.38   1.568     54
        138.75   1.550     43
        136.25   1.522     57
        134.81   1.506     42
    

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    1H NMR 399.65 MHz
    C11 H15 N 0.034 g : 0.5 ml CDCl3
    4-phenylpiperidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.296 B 7.22 C 7.19 D 3.178 E 2.734 F 2.606 G 1.97 J 1.823 K 1.642 90MHZ : HSP-03-779

         Hz     ppm     Int.
    

       2925.42   7.320    233
       2924.56   7.318    370
       2922.97   7.314    183
       2917.85   7.302    611
       2917.11   7.300    780
       2913.57   7.291     97
       2911.62   7.286    296
       2909.79   7.281    755
       2908.08   7.277    238
       2904.42   7.268     53
       2902.83   7.264     48
       2901.86   7.262     49
       2901.00   7.259     50
       2900.02   7.257     50
       2898.93   7.254     52
       2898.32   7.253     53
       2890.14   7.232    622
       2888.79   7.229   1000
       2886.96   7.224    292
       2881.59   7.211    797
       2880.86   7.209    645
       2880.37   7.208    669
       2878.78   7.204    271
       2874.88   7.194    231
       2872.92   7.189    498
       2870.85   7.184    161
       2867.19   7.175    145
       2865.84   7.171    221
       2864.38   7.168    121
       1276.00   3.193    271
       1264.04   3.163    304
       1105.59   2.767    218
       1103.15   2.761    229
       1098.88   2.750     61
       1093.38   2.736    405
       1091.06   2.731    407
       1085.69   2.717     54
       1085.08   2.716     55
       1081.18   2.706    210
       1078.86   2.700    199
       1057.37   2.646     68
       1053.71   2.637    121
       1049.93   2.628     75
       1047.85   2.622     36
       1045.29   2.616    136
       1041.63   2.607    245
       1037.96   2.598    138
       1033.20   2.586     80
       1029.54   2.577    135
       1025.88   2.567     74
        787.96   1.972    151
        736.08   1.842    265
        722.17   1.808    354
        675.05   1.690    168
        671.02   1.680    170
        667.36   1.670     43
        662.96   1.659    345
        661.99   1.657    306
        658.81   1.649    371
        650.76   1.629    244
        649.66   1.626    308
        646.61   1.618    267
        645.63   1.616    271
        637.45   1.596    108
        633.42   1.585    104
    

in CDCl3

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KBr disc

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nujol mull

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