79524-20-2

4-(4-硝基苯基)-1-丁醇(79524-20-2)核磁图(¹³CNMR)

产品名称:4-(4-硝基苯基)-1-丁醇

CAS:79524-20-2

分子式:C10H13NO3

分子量: 195.22

Mass

MS-IW-0556          
4-(p-nitrophenyl)-1-butanol
C10H13NO3           (Mass of molecular ion:    195)

   Source Temperature: 260 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      18.0       1.0
      27.0       1.5
      29.0       1.2
      30.0       3.6
      31.0       7.7
      39.0       4.4
      41.0       3.6
      50.0       1.7
      51.0       4.0
      52.0       1.5
      53.0       1.5
      55.0       1.0
      57.0       1.0
      63.0       4.0
      64.0       1.7
      65.0       4.4
      76.0       1.1
      77.0       9.5
      78.0       9.3
      79.0       2.6
      89.0      10.0
      90.0      11.1
      91.0      20.0
      92.0       3.2
     102.0       1.6
     103.0      10.3
     104.0       3.7
     105.0       1.5
     106.0       9.1
     107.0       5.7
     115.0      10.5
     116.0      19.6
     117.0       5.1
     118.0       1.6
     119.0      18.9
     120.0       5.6
     128.0       2.1
     129.0       4.6
     130.0      15.2
     131.0      11.5
     132.0       3.6
     133.0      19.0
     134.0       3.6
     135.0       2.1
     136.0       2.8
     137.0       1.3
     142.0       1.0
     145.0       1.9
     146.0       1.3
     147.0       2.1
     149.0     100.0
     150.0      10.5
     151.0       1.0
     160.0      13.7
     161.0       1.9
     162.0       1.3
     165.0       1.0
     177.0       9.3
     178.0       2.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₃ N O₃	0.05 ml : 0.5 ml CDCl₃
4-(p-nitrophenyl)-1-butanol

    Assign.     Shift(ppm)

      A             8.100
      B             7.338
      C             3.656
      D             2.748
      E             2.55
      F          1.95 to 1.40

     Hz     ppm     Int.

    732.88   8.184    133
    730.50   8.157    783
    728.56   8.135    283
    723.69   8.081    339
    721.75   8.059   1000
    719.31   8.032    171
    662.94   7.403    188
    661.13   7.382    849
    659.13   7.360    289
    654.31   7.306    279
    652.31   7.284    660
    333.88   3.729    350
    327.69   3.659    805
    321.75   3.593    322
    253.69   2.833    213
    246.56   2.754    470
    243.69   2.721    173
    239.38   2.673    319
    235.31   2.628     77
    235.00   2.624     77
    234.56   2.620     82
    228.81   2.555    685
    153.31   1.712    542
    152.56   1.704    553
    150.38   1.680    527
    148.88   1.663    612
    146.06   1.631    644

in CDCl3