83016-70-0

2-[[2-[2-(二甲氨)乙氧基乙基]甲氨基]-乙醇(83016-70-0)核磁图(¹HNMR)

产品名称:2-[[2-[2-(二甲氨)乙氧基乙基]甲氨基]-乙醇

CAS:83016-70-0

分子式:C9H22N2O2

分子量: 190.28

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-8657          
2-((2-(2-(dimethylamino)ethoxy)ethyl)methylamino)ethanol
C9H22N2O2           (Mass of molecular ion:    190)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.7
      18.0       3.8
      27.0       2.7
      28.0       5.2
      29.0       2.8
      30.0       5.2
      41.0       2.2
      42.0      19.7
      43.0       9.4
      44.0      26.0
      45.0       9.2
      54.0       1.2
      55.0       1.6
      56.0       8.4
      57.0       9.1
      58.0     100.0
      59.0       5.2
      70.0      23.6
      71.0      41.3
      72.0      34.3
      73.0       2.0
      82.0       1.7
      83.0       6.5
      84.0       1.7
      86.0       7.3
      88.0      88.2
      89.0       6.0
      90.0       2.7
     100.0       3.0
     101.0      24.1
     102.0       8.6
     114.0       1.3
     116.0       1.8
     119.0       1.3
     120.0       1.5
     159.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₂₂ N₂ O₂	0.05 ml : 0.5 ml CDCl₃
2-((2-(2-(dimethylamino)ethoxy)ethyl)methylamino)ethanol

    Assign.     Shift(ppm)

      A             4.1
      B             3.597
      C     *1      3.549
      D     *1      3.542
      E     *2      2.651
      F     *2      2.583
      G             2.502
      J             2.326
      K             2.262

     Hz     ppm     Int.

   1443.24   3.612    141
   1437.74   3.598    198
   1432.25   3.584    145
   1424.19   3.564    147
   1421.39   3.557    165
   1418.46   3.550    275
   1415.65   3.543    278
   1412.72   3.535    158
   1409.91   3.528    157
   1064.94   2.665    129
   1059.33   2.651    229
   1053.59   2.637    119
   1037.84   2.597    130
   1032.35   2.584    179
   1026.86   2.570    122
   1005.86   2.517    133
   1000.12   2.503    235
    994.38   2.489    126
    929.93   2.327    598
    903.93   2.262   1000

in CDCl3