86030-43-5

氯(二异丙基氨基)甲氧基膦(86030-43-5)Raman光谱

产品名称:氯(二异丙基氨基)甲氧基膦

CAS:86030-43-5

分子式:C7H17ClNOP

分子量: 197.64

Mass

MS-NW-9542          
methyl diisopropylphosphoramidochloridite
C7H17ClNOP          (Mass of molecular ion:    197)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       5.1
      18.0       1.1
      27.0       8.3
      28.0       4.0
      29.0       1.6
      30.0       2.3
      31.0       1.2
      36.0       1.9
      39.0       4.4
      40.0       1.0
      41.0      16.5
      42.0      21.7
      43.0      22.3
      44.0      21.0
      45.0       1.3
      46.0      16.2
      47.0      14.5
      48.0       1.3
      49.0       1.2
      50.0       5.8
      52.0       1.9
      56.0       3.0
      58.0      11.8
      59.0       1.9
      62.0       2.6
      63.0      21.2
      64.0       1.0
      67.0       1.1
      70.0       2.9
      72.0       1.9
      73.0       1.9
      74.0       1.8
      78.0      32.4
      79.0       3.4
      80.0       1.4
      82.0       2.1
      84.0      16.0
      85.0       1.2
      86.0       9.7
      88.0      40.4
      89.0       1.7
      90.0       7.9
      93.0      15.8
      94.0       2.7
      96.0       1.4
      97.0      41.4
      98.0       1.6
      99.0      13.5
     100.0       2.2
     104.0      64.7
     105.0       2.8
     108.0      33.6
     109.0       2.8
     110.0      11.6
     118.0       5.5
     120.0      21.2
     121.0       1.0
     122.0      11.3
     124.0       4.6
     126.0       1.1
     128.0       2.5
     130.0       3.0
     131.0       1.0
     132.0       3.9
     136.0       3.7
     140.0      52.5
     141.0       2.4
     142.0      17.4
     146.0       1.1
     147.0       1.5
     150.0       2.3
     152.0       2.6
     154.0       2.7
     156.0      16.5
     158.0       5.1
     162.0      80.2
     163.0       6.8
     164.0       3.9
     166.0       4.7
     168.0       2.0
     178.0       1.8
     182.0     100.0
     183.0       7.2
     184.0      33.1
     185.0       2.3
     197.0      21.5
     198.0       5.5
     199.0       7.3
     200.0       1.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₇ Cl N O P	0.05 ml : 0.5 ml CDCl₃
methyl diisopropylphosphoramidochloridite

    Assign.     Shift(ppm)

      A             3.784
      B             3.619
      C             1.26
     
     J(B,P-31)=14.2HZ

     Hz     ppm     Int.

   1531.98   3.834     66
   1531.37   3.832     64
   1526.98   3.821     30
   1524.41   3.815    113
   1520.39   3.805     75
   1517.70   3.798    160
   1513.67   3.788    123
   1510.86   3.781    134
   1508.42   3.775     65
   1506.84   3.771    149
   1504.03   3.764     75
   1500.00   3.754    112
   1493.16   3.737     51
   1456.42   3.645     62
   1453.37   3.637   1000
   1439.21   3.602   1000
    523.68   1.311    154
    516.85   1.294    255
    511.84   1.281    346
    507.45   1.270    412
    505.13   1.264    448
    503.05   1.259    461
    500.73   1.253    456
    496.34   1.242    431
    469.12   1.174     51
    462.65   1.158     34
    462.28   1.157     34

in CDCl3