91-67-8

N,N-二乙基间甲苯胺(91-67-8)质谱(MS)

产品名称:N,N-二乙基间甲苯胺

CAS:91-67-8

分子式:C11H17N

分子量: 163.26

InChI:InChI=1S/C11H17N/c1-4-12(5-2)11-8-6-7-10(3)9-11/h6-9H,4-5H2,1-3H3

InChIKey: CIPVVROJHKLHJI-UHFFFAOYSA-N

Smiles:C1(N(CC)CC)=CC=CC(C)=C1

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-0848          
N,N-diethyl-m-toluidine
C11H17N             (Mass of molecular ion:    163)

   Source Temperature: 280 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.8
      28.0       6.0
      29.0       3.3
      32.0       1.2
      39.0       3.2
      41.0       1.6
      42.0       1.1
      51.0       2.0
      63.0       1.8
      65.0       6.9
      77.0       3.7
      78.0       1.4
      79.0       1.3
      81.5       1.0
      89.0       1.9
      90.0       1.2
      91.0      17.0
      92.0       3.1
      93.0       2.8
     104.0       1.2
     105.0       1.8
     117.0       1.1
     118.0       7.8
     119.0       4.7
     120.0      27.3
     121.0       2.5
     132.0       2.2
     133.0       1.9
     134.0       3.4
     148.0     100.0
     149.0      11.2
     162.0       4.2
     163.0      34.1
     164.0       4.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₁ H₁₇ N	0.04 ml : 0.5 ml CDCl₃
N,N-diethyl-m-toluidine

    Assign.     Shift(ppm)

      A             7.174
      B             6.60
      C             6.57
      D             3.406
      E             2.383
      F             1.228

     Hz     ppm     Int.

    650.81   7.267     64
    647.25   7.228     22
    644.63   7.198     58
    642.31   7.172     78
    639.50   7.141     35
    634.94   7.090     81
    590.81   6.597    282
    583.81   6.519    107
    316.06   3.530    127
    309.00   3.451    426
    302.00   3.373    458
    295.00   3.294    159
    213.50   2.384    755
    117.06   1.308    505
    110.06   1.229   1000
    103.00   1.151    440

in CDCl3