91410-68-3

(R,R)-(+)-N,N′-双(Α-甲基苄基)磺酰胺(91410-68-3)质谱(MS)

产品名称:(R,R)-(+)-N,N′-双(Α-甲基苄基)磺酰胺

CAS:91410-68-3

分子式:C16H20N2O2S

分子量: 304.41

Mass

MS-NW-7622          
(R,R)-(+)-N,N'-bis(alpha-methylbenzyl)sulfamide
C16H20N2O2S         (Mass of molecular ion:    304)

   Source Temperature: 220 °C
   Sample Temperature: 190 °C
   Direct, 75 eV

      15.0       2.7
      18.0       1.2
      27.0       6.9
      28.0       9.4
      38.0       1.4
      39.0       6.8
      41.0       2.4
      42.0      22.5
      43.0       2.8
      44.0      10.3
      48.0       2.7
      50.0       5.5
      51.0      17.8
      52.0       4.6
      53.0       2.3
      63.0       2.8
      64.0       2.6
      65.0       4.3
      74.0       1.3
      75.0       1.5
      76.0       2.9
      77.0      37.2
      78.0      14.1
      79.0      22.9
      80.0       1.8
      89.0       1.3
      91.0       9.4
      92.0       2.4
      93.0       1.5
     102.0       1.0
     103.0      10.3
     104.0      32.7
     105.0     100.0
     106.0      71.3
     107.0       5.7
     118.0       4.0
     119.0       7.7
     120.0      29.8
     121.0       3.2
     123.0       1.2
     137.0       1.9
     168.0       2.7
     185.0      33.4
     186.0       3.2
     187.0       1.8
     199.0      14.2
     200.0       1.8
     210.0       2.7
     289.0      40.5
     290.0       7.6
     291.0       2.6

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₆ H₂₀ N₂ O₂ S	0.038 g : 0.5 ml CDCl₃
(R,R)-(+)-N,N'-bis(alpha-methylbenzyl)sulfamide

    Assign.     Shift(ppm)

      A           7.3 to 7.14
      B             4.53
      C             4.40
      D             1.453

     Hz     ppm     Int.

    655.31   7.317     70
    653.81   7.301     92
    653.50   7.297     94
    652.56   7.287    143
    651.25   7.272    161
    650.81   7.267    154
    649.19   7.249    498
    647.38   7.229    501
    646.13   7.215    543
    645.06   7.203   1000
    643.06   7.181    716
    639.81   7.144    232
    638.50   7.130    135
    636.88   7.112     98
    634.88   7.089    114
    633.31   7.072     65
    409.56   4.574     88
    409.13   4.569     90
    408.88   4.566     90
    408.56   4.562     90
    408.06   4.557     93
    406.56   4.540    113
    405.94   4.533    112
    405.56   4.529    112
    402.63   4.496     86
    400.38   4.471    164
    396.13   4.424     53
    393.94   4.399    178
    387.50   4.327    115
    133.50   1.491    777
    130.00   1.452    133
    126.94   1.418    746
    122.56   1.369     57

in CDCl3