932-96-7

4-氯-N-甲基苯胺(932-96-7)核磁图(¹³CNMR)

产品名称:4-氯-N-甲基苯胺

CAS:932-96-7

分子式:C7H8ClN

分子量: 141.6

InChI:InChI=1S/C7H8ClN/c1-9-7-4-2-6(8)3-5-7/h2-5,9H,1H3

InChIKey: XCEYKKJMLOFDSS-UHFFFAOYSA-N

Smiles:C1(NC)=CC=C(Cl)C=C1

Mass

MS-IW-1327          
p-chloro-N-methylaniline
C7H8ClN             (Mass of molecular ion:    141)

   Source Temperature: 240 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      28.0       1.5
      30.0       1.2
      38.0       1.0
      39.0       1.4
      50.0       3.0
      51.0       2.8
      52.0       1.9
      52.5       1.7
      62.0       1.5
      63.0       3.6
      64.0       1.8
      65.0       2.1
      70.0       2.9
      70.5       3.3
      71.0       1.2
      71.5       1.0
      73.0       2.7
      74.0       2.4
      75.0       7.2
      76.0       1.7
      77.0      14.3
      78.0       2.1
      79.0       1.3
      90.0       2.0
      91.0       1.7
      99.0       7.3
     100.0       1.2
     101.0       2.4
     104.0       5.1
     105.0       9.5
     106.0       2.8
     111.0       6.4
     112.0       5.3
     113.0       4.5
     114.0       1.9
     126.0       3.2
     127.0       5.2
     128.0       1.3
     129.0       1.5
     138.0       3.2
     139.0       1.2
     140.0     100.0
     141.0      88.8
     142.0      38.4
     143.0      28.7
     144.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₈ Cl N	0.05 ml : 0.5 ml CDCl₃
p-chloro-N-methylaniline

    Assign.     Shift(ppm)

      A             7.087
      B             6.446
      C             3.
      D             2.715

     Hz     ppm     Int.

   2840.45   7.108     62
   2837.16   7.100    478
   2834.96   7.094    178
   2833.01   7.089     24
   2832.28   7.087     24
   2830.44   7.083    185
   2828.25   7.077    486
   2824.95   7.069     76
   2583.98   6.466     60
   2580.69   6.458    445
   2578.49   6.452    160
   2573.97   6.441    155
   2571.78   6.436    413
   2568.48   6.427     59
   1433.96   3.589     20
   1085.08   2.716   1000

in CDCl3